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DRUMS OILY SLUDGE #4 SAMPLE RESULTS - 04 <br /> Collected date/time: 08/11/21 07:00 L1391519 <br /> Volatile Organic Compounds (GC/MS) by Method 82608 <br /> Result Qualifier MDL RDL Dilution Analysis Batch Cp <br /> Analyte mg/kg mg/kg mg/kg date/time <br /> 1,2,4-Trimethyl benzene 0.312 0.00638 0.0202 4.04 08/23/202116:32 WG1727785 FTc <br /> 1,2,3-Trimethyl benzene 0.230 0.00638 0.0202 4.04 08/23/202116:32 WG1727785 <br /> 1,3,5-Trimethyl benzene 0.0650 0.00808 0.0202 4.04 08/23/202116:32 WG1727785 FSS <br /> Vinyl chloride U 0.00469 0.0101 4.04 08/23/202116:32 WG1727785 <br /> Xylenes,Total 0.186 0.00356 0.0263 4.04 08/23/202116:32 WG1727785 <br /> (S)Toluene-d8 111 75.0-131 08/23/20211632 WG1727785 4Cn <br /> (S)4-Bromofluorobenzene 87.4 67.0-138 08/23/202116:32 WG1727785 <br /> (S)1,2-Dich/oroethone-d4 90.4 70.0-130 08/23/202116:32 WG1727785 <br /> Semi-Volatile Organic Compounds (GC) by Method 8015 <br /> FResult Qualifier MDL RDL Dilution Analysis Batch <br /> Analyte mg/kg mg/kg mg/kg date/time <br /> C12-C22 Hydrocarbons 2660 367 2000 500 08/26/202108:44 WG1727935 AGI <br /> C22-02 Hydrocarbons 32600 665 2000 500 08/26/202108:44 WG1727935 <br /> C32-C40 Hydrocarbons 13800 665 2000 500 08/26/202108:44 WG1727935 rAl(S)o-Terpheny/ 0.000 J7 18.0-148 08/26/202108:44 WG1727935 <br /> Semi Volatile Organic Compounds (GC/MS) by Method 8270C [ScResult Qualifier MDL RDL Dilution Analysis Batch <br /> Analyte mg/kg mg/kg mg/kg date/time <br /> Acenaphthene U 0.539 3.33 100 08/24/202120:14 WG1727513 <br /> Acenaphthylene U 0.469 3.33 100 08/24/202120:14 WG1727513 <br /> Anthracene U 0.593 3.33 100 08/24/202120:14 WG1727513 <br /> Benzidine U 6.26 167 100 08/24/202120:14 WG1727513 <br /> Benzo(a)anthracene U 0.587 3.33 100 08/24/202120:14 WG1727513 <br /> Benzo(b)fluoranthene U 0.621 3.33 100 08/24/202120:14 WG1727513 <br /> Benzo(k)fluoranthene U 0.592 3.33 100 08/24/202120:14 WG1727513 <br /> Benzo(g,h,i)perylene U 0.609 3.33 100 08/24/202120:14 WG1727513 <br /> Benzo(a)pyrene U 0.619 3.33 100 08/24/202120:14 WG1727513 <br /> Bis(2-chlorethoxy)methane U 1.00 33.3 100 08/24/202120:14 WG1727513 <br /> Bis(2-chloroethyl)ether U 1.10 33.3 100 08/24/202120:14 WG1727513 <br /> 2,2-Oxybis(1-Chloropropane) U 1.44 33.3 100 08/24/202120:14 WG1727513 <br /> 4-Bromophenyl-phenylether U 1.17 33.3 100 08/24/202120:14 WG1727513 <br /> 2-Chloronaphthalene U 0.585 3.33 100 08/24/202120:14 WG1727513 <br /> 4-Chlorophenyl-phenylether U 1.16 33.3 100 08/24/202120:14 WG1727513 <br /> Chrysene U 0.662 3.33 100 08/24/202120:14 WG1727513 <br /> Dibenz(a,h)anthracene U 0.923 3.33 100 08/24/202120:14 WG1727513 <br /> 3,3-Dichlorobenzidine U 1.23 33.3 100 08/24/202120:14 WG1727513 <br /> 2,4-Dinitrotoluene U 0.955 33.3 100 08/24/202120:14 WG1727513 <br /> 2,6-Dinitrotoluene U 1.09 33.3 100 08/24/202120:14 WG1727513 <br /> Fluoranthene 0.942 J 0.601 3.33 100 08/24/202120:14 WG1727513 <br /> Fluorene U 0.542 3.33 100 08/24/202120:14 WG1727513 <br /> Hexachlorobenzene U 1.18 33.3 100 08/24/202120:14 WG1727513 <br /> Hexachloro-1,3-butadiene U 1.12 33.3 100 08/24/202120:14 WG1727513 <br /> Hexachlorocyclopentadiene U 1.75 33.3 100 08/24/202120:14 WG1727513 <br /> Hexachloroethane U 1.31 33.3 100 08/24/202120:14 WG1727513 <br /> Indeno(1,2,3-cd)pyrene U 0.941 3.33 100 08/24/202120:14 WG1727513 <br /> Isophorone U 1.02 33.3 100 08/24/202120:14 WG1727513 <br /> Naphthalene 0.841 J 0.836 3.33 100 08/24/202120:14 WG1727513 <br /> Nitrobenzene U 1.16 33.3 100 08/24/202120:14 WG1727513 <br /> n-Nitrosodimethyla mine U 4.94 33.3 100 08/24/202120:14 WG1727513 <br /> n-Nitrosodiphenyla mine U 2.52 33.3 100 08/24/202120:14 WG1727513 <br /> n-Nitrosodi-n-propylamine U 1.11 33.3 100 08/24/202120:14 WG1727513 <br /> Phenanthrene 0.813 J 0.661 3.33 100 08/24/202120:14 WG1727513 <br /> Benzylbutyl phthalate U 1.04 33.3 100 08/24/202120:14 WG1727513 <br /> ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: <br /> UPRR-American Integrated Services,Inc AIS 81046-16 L1391519 08/27/2109:46 19 of 44 <br />