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QC Sample Results C <br /> Client: Union Pacific Railroad Job ID: 720-92832-1 <br /> Project/Site: UPRR-Stockton Monthly& Semi Annual <br /> Method: 625 - Semivolatile Organic Compounds (GC/MS) (Continued) <br /> Lab Sample ID: LCS 440-545413/2-A Client Sample ID: Lab Control Sample <br /> Matrix: Water Prep Type: Total/NA <br /> Analysis Batch: 545900 Prep Batch: 545413 <br /> Spike LCS LCS %Rec. <br /> Analyte Added Result Qualifier Unit D %Rec Limits <br /> Benzo[g,h,i]perylene 100 95.1 ug/L 95 10-150 <br /> Benzo[k]fluoranthene 100 100 ug/L 100 11-150 <br /> Benzoic acid 100 73.4 ug/L 73 40-100 <br /> Benzyl alcohol 100 93.1 ug/L 93 49-102 <br /> Bis(2-chloroethoxy)methane 100 99.1 ug/L 99 33-150 <br /> Bis(2-chloroethyl)ether 100 97.0 ug/L 97 12-150 ' <br /> bis(2-chloroisopropyl)ether 100 97.9 ug/L 98 44-103 <br /> Bis(2-ethylhexyl)phthalate 100 96.0 ug/L 96 10-150 <br /> Butyl benzyl phthalate 100 91.7 ug/L 92 10-150 <br /> Chrysene 100 97.2 ug/L 97 17-150 <br /> Di-n-butyl phthalate 100 98.2 ug/L 98 10-118 <br /> Di-n-octyl phthalate 100 85.4 ug/L 85 10-146 <br /> Dibenz(a,h)anthracene 100 97.2 ug/L 97 10-150 <br /> Dibenzofuran 100 97.1 ug/L 97 52-105 <br /> Diethyl phthalate 100 98.7 ug/L 99 10-114 <br /> Dimethyl phthalate 100 96.7 ug/L 97 10-112 ❑ <br /> Fluoranthene 100 102 ug/L 102 26-137 <br /> Fluorene 100 102 ug/L 102 59-121 <br /> Hexachlorobenzene 100 98.5 ug/L 98 10-150 <br /> Hexachlorobutadiene 100 78.2 ug/L 78 24-116 <br /> Hexachlorocyclopentadiene 100 42.0 ug/L 42 20-67 <br /> Hexachloroethane 100 72.8 ug/L 73 40-113 <br /> Indeno[1,2,3-cd]pyrene 100 88.8 ug/L 89 10-150 <br /> Isophorone 100 104 ug/L 104 21-150 <br /> N-Nitrosodi-n-propylamine 100 115 ug/L 115 10-150 <br /> N-Nitrosodiphenylamine 100 100 ug/L 100 54-111 <br /> Naphthalene 100 89.2 ug/L 89 21-133 <br /> Nitrobenzene 100 96.0 ug/L 96 35-150 <br /> Pentachlorophenol 200 205 ug/L 103 14-150 <br /> Phenanthrene 100 96.9 ug/L 97 54-120 <br /> Phenol 100 97.1 ug/L 97 10-112 <br /> Pyrene 100 91.9 ug/L 92 52-115 <br /> LCS LCS <br /> Surrogate %Recovery Qualifier Limits <br /> 2-Fluorobiphenyl 89 50-120 <br /> 2-Fluorophenol 75 30-120 <br /> 2,4,6-Tribromophenol 100 40-120 <br /> Nitrobenzene-d5 92 45-120 <br /> Terphenyl-d 14 101 10-150 <br /> Phenol-d6 90 35-120 <br /> Lab Sample ID: LCSD 440-545413/3-A Client Sample ID: Lab Control Sample Dup <br /> Matrix: Water Prep Type: Total/NA <br /> Analysis Batch: 545900 Prep Batch: 545413 <br /> Spike LCSD LCSD %Rec. RPD <br /> Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> 1,2,4-Trichlorobenzene 100 74.4 ug/L 74 44-142 15 35 <br /> 1,2-Dichlorobenzene 100 70.7 ug/L 71 32-129 12 35 <br /> Eurofins TestAmerica, Pleasanton <br /> Page 16 of 31 5/20/2019 <br />