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QC Sample Results Client: Union Pacific Railroad Job ID: 720-92832-1 Project/Site: UPRR-Stockton Monthly& Semi Annual Method: 625 - Semivolatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCSD 440-545413/3-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 545900 Prep Batch: 545413 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit 1,2-Diphenylhydrazine(as 100 91.4 ug/L 91 55-106 15 35 Azobenzene) 1,3-Dichlorobenzene 100 67.6 ug/L 68 10-150 14 35 1,4-Dichlorobenzene 100 70.3 ug/L 70 20-124 11 35 2,4,5-Trichlorophenol 100 75.6 ug/L 76 54-101 14 35 2,4,6-Trichlorophenol 100 86.3 ug/L 86 37-144 14 35 2,4-Dichlorophenol 100 84.1 ug/L 84 39-135 13 35 2,4-Dimethylphenol 100 71.5 ug/L 72 32-119 17 35 2,4-Dinitrophenol 200 159 ug/L 80 50-150 13 35 2,4-Dinitrotoluene 100 83.9 ug/L 84 39-139 14 35 2,6-Dinitrotoluene 100 83.3 ug/L 83 50-150 16 35 2-Chloronaphthalene 100 77.7 ug/L 78 60-118 12 35 2-Chlorophenol 100 75.4 ug/L 75 23-134 12 35 2-Methylnaphthalene 100 83.2 ug/L 83 46-93 12 35 2-Methylphenol 100 86.3 ug/L 86 47-97 13 35 2-Nitroaniline 100 89.8 ug/L 90 54-108 16 35 2-Nitrophenol 100 78.5 ug/L 78 29-150 12 35 3,3'-Dichlorobenzidine 100 76.0 ug/L 76 4-150 13 35 3-Nitroaniline 100 67.0 ug/L 67 60-110 13 35 4,6-Dinitro-2-methylphenol 200 185 ug/L 92 10-150 15 35 4-Bromophenyl phenyl ether 100 84.2 ug/L 84 53-127 16 35 4-Chloro-3-methylphenol 100 89.0 ug/L 89 22-147 16 35 4-Chloroaniline 100 69.8 ug/L 70 53-100 8 35 4-Chlorophenyl phenyl ether 100 89.1 ug/L 89 25-150 13 35 3-Methylphenol+4-Methylphenol 100 89.3 ug/L 89 49-100 14 35 4-Nitroaniline 100 84.0 ug/L 84 59-111 15 35 4-Nitrophenol 200 150 ug/L 75 10-132 20 35 Acenaphthene 100 80.8 ug/L 81 47-145 13 35 Acenaphthylene 100 80.6 ug/L 81 33-145 15 35 Aniline 100 85.6 ug/L 86 33-108 9 35 Anthracene 100 84.9 ug/L 85 27-133 14 35 Benzidine 100 24.3 J" ug/L 24 5-137 48 35 Benzo[a]anthracene 100 84.1 ug/L 84 33-143 15 35 Benzo[a]pyrene 100 76.0 ug/L 76 17-150 13 35 Benzo[b]fluoranthene 100 80.0 ug/L 80 24-150 16 35 Benzo[g,h,i]perylene 100 83.4 ug/L 83 10-150 13 35 Benzo[k]fluoranthene 100 82.5 ug/L 82 11-150 19 35 Benzoic acid 100 59.3 ug/L 59 40-100 21 35 Benzyl alcohol 100 80.0 ug/L 80 49-102 15 35 Bis(2-chloroethoxy)methane 100 84.9 ug/L 85 33-150 16 35 Bis(2-chloroethyl)ether 100 83.4 ug/L 83 12-150 15 35 bis(2-chloroisopropyl)ether 100 86.6 ug/L 87 44-103 12 35 Bis(2-ethylhexyl)phthalate 100 82.4 ug/L 82 10-150 15 35 Butyl benzyl phthalate 100 77.3 ug/L 77 10-150 17 35 Chrysene 100 84.2 ug/L 84 17-150 14 35 Di-n-butyl phthalate 100 85.2 ug/L 85 10-118 14 35 Di-n-octyl phthalate 100 74.2 ug/L 74 10-146 14 35 Dibenz(a,h)anthracene 100 85.8 ug/L 86 10-150 12 35 Dibenzofuran 100 83.5 ug/L 84 52-105 15 35 Eurofins TestAmerica, Pleasanton Page 17 of 31 5/20/2019