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None ug/Kg Tentatively Identified Compound <br />Analyzed <br />02/06/20 13:20 <br />02/06/20 13:20 <br />02/06/20 13:20 <br />02/06/20 13:20 <br />02/06/20 13:20 <br />02/06/20 13:20 <br />Prepared <br />02/05/20 12:25 <br />02/05/20 12:25 <br />02/05/20 12:25 <br />02/05/20 12:25 <br />02/05/20 12:25 <br />02/05/20 12:25 <br />Lab Sample ID: MB 180-306131/1-A <br />Matrix: Solid <br />Analysis Batch: 306266 <br />MB MB <br />Analyte Result Qualifier <br />1,2,4-Trichlorobenzene ND 10000 <br />2,4,5-Trichlorophenol ND 10000 <br />2,4,6-Trichlorophenol ND 10000 <br />MB MB <br />Tentatively Identified Compound Est. Result Qualifier Unit <br />MB <br />Qualifier Limits <br />2-Fluorobiphenyl <br />2-Fluorophenol <br />Nitrobenzene-d5 <br />Phenol-d5 <br />Terphenyl-d14 <br />2,4,6-Tribromophenol <br />Client Sample ID: Method Blank <br />Prep Type: Total/NA <br />Prep Batch: 306131 <br />CAS No. Prepared Analyzed <br />D Prepared Analyzed <br />02/05/20 12:25 02/06/20 13:20 <br />02/05/20 12:25 02/06/20 13:20 <br />02/05/20 12:25 02/06/20 13:20 <br />Dil Fac <br />1 <br />1 <br />1 <br />Dil Fac <br />1 <br />Dil Fac <br />Lab Sample ID: LCS 180-306131/2-A <br />Matrix: Solid <br />Analysis Batch: 306266 <br />Analyte <br />Spike <br />Added <br />LCS LCS <br />Result Qualifier <br />Client Sample ID: Lab Control Sample <br />Prep Type: Total/NA <br />Prep Batch: 306131 <br />%Rec. <br />Unit D %Rec Limits <br />Acenaphthene 100000 95300 ug/Kg 95 47 - 104 <br />Acenaphthylene 100000 98500 ug/Kg 99 49 _ 114 <br />Anthracene 100000 97600 ug/Kg 98 45 - 112 <br />Benzo[a]anthracene 100000 95600 ug/Kg 96 47- 110 <br />Benzo[a]pyrene 100000 95400 ug/Kg 95 40 - 112 <br />Benzo[b]fluoranthene 100000 84700 ug/Kg 85 41 107 <br />Benzo[g,h,i]perylene 100000 101000 ug/Kg 01 38 - 126 <br />Benzo[k]fluoranthene 100000 96400 ug/Kg 96 40 - 115 <br />Bis(2-chloroethoxy)methane 100000 95400 ug/Kg 95 38 - 105 <br />Bis(2-chloroethyl)ether 100000 90700 ug/Kg 91 35 - 106 <br />Bis(2-ethylhexyl) phthalate 100000 105000 ug/Kg 05 40 _ 117 <br />4-Bromophenyl phenyl ether 100000 99900 ug/Kg 00 47- 110 <br />Butyl benzyl phthalate 100000 105000 ug/Kg 05 35 - 118 <br />Carbazole 100000 95800 ug/Kg 96 45 - 114 <br />4-Chloroaniline 100000 91600 ug/Kg 92 25 - 108 <br />4-Chloro-3-methylphenol 100000 92700 ug/Kg 93 40 _ 109 <br />2-Chloronaphthalene 100000 97700 ug/Kg 98 46 - 101 <br />2-Chlorophenol 100000 91600 ug/Kg 92 40 - 101 <br />4-Chlorophenyl phenyl ether 100000 95000 ug/Kg 95 47 _ 109 <br />Chrysene 100000 90700 ug/Kg 91 46- 111 <br />Dibenz(a,h)anthracene 100000 93900 ug/Kg 94 39 - 127 <br />Dibenzofuran 100000 92700 ug/Kg 93 46 - 104 <br />1,2-Dichlorobenzene 100000 89400 ug/Kg 89 36 - 101 <br />1,3-Dichlorobenzene 100000 90600 ug/Kg 91 35 - 101 <br />1,4-Dichlorobenzene 100000 90300 ug/Kg 90 36 - 101 <br />3,3'-Dichlorobenzidine 100000 87100 ug/Kg 87 25 - 122 <br />2,4-Dichlorophenol 100000 98600 ug/Kg 99 47 _ 105 <br />Diethyl phthalate 100000 97200 ug/Kg 97 47 - 115 <br />ug/Kg <br />ug/Kg <br />ug/Kg <br />RT <br />RL Unit <br />Surrogate <br />MB <br />%Recovery <br />86 <br />77 <br />85 <br />79 <br />105 <br />73 <br />35- 105 <br />39-103 <br />25-104 <br />25 -105 <br />25 -127 <br />35 -124 <br />02/05/20 12:25 02/06/20 13.20 <br />QC Sample Results <br />Client: Calgon Carbon Corporation Job ID: 180-101877-6 <br />Project/Site: Carbon Acceptance, 20200149.1 <br />Method: EPA 82700 - Semivolatile Organic Compounds (GC/MS) (Continued) <br />Eurofins TestAmerica, Pittsburgh <br />Page 14 of 20 2/17/2020