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QC Sample Results <br />Client: Calgon Carbon Corporation Job ID: 180-101877-6 <br />Project/Site: Carbon Acceptance, 20200149.1 <br />Method: EPA 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) <br />Lab Sample ID: LCS 180-306131/2-A <br />Matrix: Solid <br />Analysis Batch: 306266 <br />Analyte <br />Spike <br />Added <br />LCS LCS <br />Result Qualifier <br />Client Sample ID: Lab Control Sample <br />Prep Type: Total/NA <br />Prep Batch: 306131 <br />%Rec. <br />Unit D %Rec Limits <br />2,4-Dimethylphenol 100000 94700 ug/Kg 95 44 _ 105 <br />Dim ethyl phthalate 100000 97400 ug/Kg 97 49- 111 <br />Di-n-butyl phthalate 100000 102000 ug/Kg 102 43 - 121 <br />4,6-Dinitro-2-methylphenol 200000 151000 ug/Kg 76 24 - 134 <br />2,4-Dinitrophenol 200000 104000 ug/Kg 52 10 - 146 <br />2,4-Dinitrotoluene 100000 97300 ug/Kg 97 45 - 124 <br />2,6-Dinitrotoluene 100000 100000 ug/Kg 100 40 - 122 <br />Di-n-octyl phthalate 100000 101000 ug/Kg 101 33 - 129 <br />Fluoranthene 100000 96700 ug/Kg 97 40- 120 <br />Fluorene 100000 94900 ug/Kg 95 46 _ 109 <br />Hexachlorobenzene 100000 91900 ug/Kg 92 47 - 108 <br />Hexachlorobutadiene 100000 98200 ug/Kg 98 43 - 107 <br />Hexachlorocyclopentadiene 100000 107000 ug/Kg 107 23- 129 <br />Hexachloroethane 100000 92300 ug/Kg 92 35 _ 104 <br />Indeno[1,2,3-cd]pyrene 100000 108000 ug/Kg 108 41 -125 <br />Isophorone 100000 92700 ug/Kg 93 40 _ 110 <br />2-Methylnaphthalene 100000 93000 ug/Kg 93 45 _ 100 <br />2-Methylphenol 100000 91300 ug/Kg 91 40 - 104 <br />Methylphenol, 3 & 4 100000 93000 ug/Kg 93 40- 114 <br />Naphthalene 100000 93900 ug/Kg 94 38- 105 <br />2-Nitroaniline 100000 101000 ug/Kg 101 45 - 117 <br />3-Nitroaniline 100000 93200 ug/Kg 93 34 - 122 <br />4-Nitroaniline 100000 96500 ug/Kg 97 38 - 123 <br />Nitrobenzene 100000 92700 ug/Kg 93 33- 109 <br />2-Nitrophenol 100000 95100 ug/Kg 95 40 - 106 <br />4-Nitrophenol 200000 197000 ug/Kg 98 36 - 127 <br />N-Nitrosodi-n-propylamine 100000 87800 ug/Kg 88 42 - 107 <br />N-Nitrosodiphenylamine 100000 99000 ug/Kg 99 44 _ 111 <br />2,2'-oxybis[1-chloropropane] 100000 76600 ug/Kg 77 31 - 111 <br />Pentachlorophenol 200000 163000 ug/Kg 82 17- 122 <br />Phenanthrene 100000 92900 ug/Kg 93 43 _ 108 <br />Phenol 100000 90100 ug/Kg 90 41 - 102 <br />Pyrene 100000 96900 ug/Kg 97 41 - 115 <br />1,2,4-Trichlorobenzene 100000 94800 ug/Kg 95 43 - 100 <br />2,4,5-Trichlorophenol 100000 103000 ug/Kg 103 42 _ 112 <br />2,4,6-Trichlorophenol 100000 100000 ug/Kg 100 45 - 106 <br />LCS LCS <br />Surrogate %Recovery Qualifier Limits <br />2-Fluorobtphenyl 97 35 - 105 <br />2-Fluorophenol 88 39-103 <br />Nitrobenzene-d5 96 25-104 <br />Phenol-d5 90 25-105 <br />Terphenyl-d14 105 25-127 <br />2,4,6-Tribromophenol 95 35-124 <br />Eurofins TestAmerica, Pittsburgh <br />Page 15 of 20 2/17/2020