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Quality Control Report <br />McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701 <br />Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 <br />http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts" <br />Client:Clean Harbors <br />Project:Turner Cut <br />Date Analyzed:03/01/2025 <br />Date Prepared:03/01/2025 <br />WorkOrder:2502J06 <br />BatchID:312478 <br />Analytical Method:SW8260D <br />Unit:µg/L <br />Sample ID:MB/LCS/LCSD-312478 <br />Instrument:GC45 <br />Matrix:Water <br />Extraction Method:SW5030B <br />QC Summary Report for SW8260D <br />Analyte MB <br />Result <br />MDL RL SPK <br />Val <br />MB IS/SS <br />%REC <br />MB IS/SS <br />Limits <br />Acetone ND 6.7 40 --- <br />tert-Amyl methyl ether (TAME)ND 0.13 0.50 --- <br />Benzene ND 0.035 0.20 --- <br />Bromobenzene ND 0.11 0.50 --- <br />Bromochloromethane ND 0.21 0.50 --- <br />Bromodichloromethane ND 0.035 0.050 --- <br />Bromoform ND 0.24 0.50 --- <br />Bromomethane ND 0.25 0.50 --- <br />2-Butanone (MEK)ND 1.4 5.0 --- <br />t-Butyl alcohol (TBA)ND 1.5 5.0 --- <br />n-Butyl benzene ND 0.16 0.50 --- <br />sec-Butyl benzene ND 0.10 0.50 --- <br />tert-Butyl benzene ND 0.17 0.50 --- <br />Carbon Disulfide ND 0.12 0.50 --- <br />Carbon Tetrachloride ND 0.034 0.050 --- <br />Chlorobenzene ND 0.095 0.50 --- <br />Chloroethane ND 0.25 0.50 --- <br />Chloroform ND 0.043 0.10 --- <br />Chloromethane ND 0.16 0.50 --- <br />2-Chlorotoluene ND 0.12 0.50 --- <br />4-Chlorotoluene ND 0.099 0.50 --- <br />Dibromochloromethane ND 0.073 0.15 --- <br />1,2-Dibromo-3-chloropropane ND 0.0079 0.020 --- <br />1,2-Dibromoethane (EDB)ND 0.016 0.040 --- <br />Dibromomethane ND 0.17 0.50 --- <br />1,2-Dichlorobenzene ND 0.10 0.50 --- <br />1,3-Dichlorobenzene ND 0.14 0.50 --- <br />1,4-Dichlorobenzene ND 0.089 0.50 --- <br />Dichlorodifluoromethane ND 0.16 0.50 --- <br />1,1-Dichloroethane ND 0.14 0.50 --- <br />1,2-Dichloroethane (1,2-DCA)ND 0.0093 0.020 --- <br />1,1-Dichloroethene ND 0.0058 0.010 --- <br />cis-1,2-Dichloroethene ND 0.14 0.50 --- <br />trans-1,2-Dichloroethene ND 0.15 0.50 --- <br />1,2-Dichloropropane ND 0.039 0.10 --- <br />1,3-Dichloropropane ND 0.16 0.50 --- <br />2,2-Dichloropropane ND 0.17 0.50 --- <br />1,1-Dichloropropene ND 0.11 0.50 --- <br />CA ELAP 1644 • NELAP 4033ORELAP <br />(Cont.) <br />Page 19 of 34