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Quality Control Report <br />McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701 <br />Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 <br />http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts" <br />Client:Clean Harbors <br />Project:Turner Cut <br />Date Analyzed:03/01/2025 <br />Date Prepared:03/01/2025 <br />WorkOrder:2502J06 <br />BatchID:312478 <br />Analytical Method:SW8260D <br />Unit:µg/L <br />Sample ID:MB/LCS/LCSD-312478 <br />Instrument:GC45 <br />Matrix:Water <br />Extraction Method:SW5030B <br />QC Summary Report for SW8260D <br />Analyte MB <br />Result <br />MDL RL SPK <br />Val <br />MB IS/SS <br />%REC <br />MB IS/SS <br />Limits <br />cis-1,3-Dichloropropene ND 0.13 0.50 --- <br />trans-1,3-Dichloropropene ND 0.20 0.50 --- <br />Diisopropyl ether (DIPE)ND 0.16 0.50 --- <br />Ethylbenzene ND 0.10 0.50 --- <br />Ethyl tert-butyl ether (ETBE)ND 0.15 0.50 --- <br />Freon 113 ND 0.15 0.50 --- <br />Hexachlorobutadiene ND 0.064 0.50 --- <br />Hexachloroethane ND 0.078 0.20 --- <br />2-Hexanone ND 0.23 0.50 --- <br />Isopropylbenzene ND 0.10 0.50 --- <br />4-Isopropyl toluene ND 0.19 0.50 --- <br />Methyl-t-butyl ether (MTBE)ND 0.15 0.50 --- <br />Methylene chloride ND 1.5 2.0 --- <br />4-Methyl-2-pentanone (MIBK)ND 0.22 0.50 --- <br />Naphthalene ND 0.17 0.30 --- <br />n-Propyl benzene ND 0.11 0.50 --- <br />Styrene ND 0.22 2.0 --- <br />1,1,1,2-Tetrachloroethane ND 0.086 0.50 --- <br />1,1,2,2-Tetrachloroethane ND 0.015 0.020 --- <br />Tetrachloroethene ND 0.036 0.20 --- <br />Toluene ND 0.10 0.50 --- <br />1,2,3-Trichlorobenzene ND 0.17 0.50 --- <br />1,2,4-Trichlorobenzene ND 0.13 0.50 --- <br />1,1,1-Trichloroethane ND 0.13 0.50 --- <br />1,1,2-Trichloroethane ND 0.032 0.10 --- <br />Trichloroethene ND 0.034 0.10 --- <br />Trichlorofluoromethane ND 0.14 0.50 --- <br />1,2,3-Trichloropropane ND 0.0036 0.0050 --- <br />1,2,4-Trimethylbenzene ND 0.10 0.50 --- <br />1,3,5-Trimethylbenzene ND 0.096 0.50 --- <br />Vinyl Chloride ND 0.0044 0.0050 --- <br />m,p-Xylene ND 0.22 1.0 --- <br />o-Xylene ND 0.12 0.50 --- <br />CA ELAP 1644 • NELAP 4033ORELAP <br />(Cont.) <br />Page 20 of 34