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Pace Analytical Services,LLC <br /> ® 1700 Elm Street-Suite 200 <br /> laceAnalytical Minneapolis,MN 55414 <br /> www.pacelabs.com (612)607-1700 <br /> ANALYTICAL RESULTS <br /> Project: 7036 French Camp CA-Lathrop In-Revised Report <br /> Pace Project No.: 10508446 <br /> Sample: SS-3-14 Lab ID: 10508446005 Collected: 02/10/20 11:26 Received: 02/13/20 10:50 Matrix: Solid <br /> Results reported on a"wet-weight'basis <br /> Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual <br /> 8015 GCS THC-Diesel Analytical Method:EPA 8015 Modified Preparation Method: EPA 3550 Sonication <br /> Motor Oil Range(C24-C36) 10.8 mg/kg 9.8 1 02/13/20 15:38 02/17/20 19:21 N2 <br /> TPH-DRO(C10-C28) ND mg/kg 9.8 1 02/13/20 15:38 02/17/20 19:21 <br /> Surrogates <br /> o-Terphenyl(S) 82 %. 30-146 1 02/13/20 15:38 02/17/20 19:21 84-15-1 <br /> n-Triacontane(S) 72 %. 30-144 1 02/13/20 15:38 02/17/20 19:21 638-68-6 <br /> Sample: SS-4-12 Lab ID: 10508446007 Collected: 02/10/20 11:48 Received: 02/13/20 10:50 Matrix: Solid <br /> Results reported on a"wet-weight'basis <br /> Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual <br /> 8015 GCS THC-Diesel Analytical Method:EPA 8015 Modified Preparation Method:EPA 3550 Sonication <br /> Motor Oil Range(C24-C36) 872 mg/kg 491 50 02/13/20 15:38 02/17/20 20:19 N2 <br /> TPH-DRO(C10-C28) 8110 mg/kg 491 50 02/13/20 15:38 02/17/20 20:19 <br /> Surrogates <br /> o-Terphenyl(S) 0 %. 30-146 50 02/13/20 15:38 02/17/20 20:19 84-15-1 S4 <br /> n-Triacontane(S) 0 %. 30-144 50 02/13/20 15:38 02/17/20 20:19 638-68-6 S4 <br /> Sample: SS-4-40 Lab ID: 10508446008 Collected: 02/10/20 12:11 Received: 02/13/20 10:50 Matrix: Solid <br /> Results reported on a"wet-weight'basis <br /> Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[ <br /> 8015 GCS THC-Diesel Analytical Method:EPA 8015 Modified Preparation Method:EPA 3550 Sonication <br /> Motor Oil Range(C24-C36) 212 mg/kg 49.7 5 02/13/20 15:38 02/17/20 20:53 N2 <br /> TPH-DRO(C10-C28) 566 mg/kg 49.7 5 02/13/20 15:38 02/17/20 20:53 <br /> Surrogates <br /> o-Terphenyl(S) 102 %. 30-146 5 02/13/20 15:38 02/17/20 20:53 84-15-1 <br /> n-Triacontane(S) 82 %. 30-144 5 02/13/20 15:38 02/17/20 20:53 638-68-6 <br /> Sample: SS-5-14 Lab ID: 10508446009 Collected: 02/10/20 12:54 Received: 02/13/20 10:50 Matrix: Solid <br /> Results reported on a"wet-weight'basis <br /> Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual <br /> 8015 GCS THC-Diesel Analytical Method:EPA 8015 Modified Preparation Method:EPA 3550 Sonication <br /> Motor Oil Range(C24-C36) 1060 mg/kg 198 20 02/13/20 15:38 02/17/20 20:30 N2 <br /> TPH-DRO(C10-C28) 4860 mg/kg 198 20 02/13/20 15:38 02/17/20 20:30 <br /> Surrogates <br /> o-Terphenyl(S) 0 %. 30-146 20 02/13/20 15:38 02/17/20 20:30 84-15-1 S4 <br /> n-Triacontane(S) 0 %. 30-144 20 02/13/20 15:38 02/17/20 20:30 638-68-6 S4 <br /> REPORT OF LABORATORY ANALYSIS <br /> This report shall not be reproduced,except in full, <br /> Date:03/20/2020 02:52 PM without the written consent of Pace Analytical Services,LLC. Page 10 of 39 <br />