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Pace Analytical Services,LLC <br /> acmnalytical a 1700 Elm Street-Suite 200 <br /> Minneapolis,MN 55414 <br /> www.pacelabs.com <br /> (612)607-1700 <br /> ANALYTICAL RESULTS <br /> Project: 7036 French Camp CA-Lathrop In-Revised Report <br /> Pace Project No.: 10508446 <br /> Sample: SS-5-49 Lab ID: 10508446010 Collected: 02/10/20 13:20 Received: 02/13/20 10:50 Matrix: Solid <br /> Results reported on a"wet-weight"basis <br /> Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual <br /> 8015 GCS THC-Diesel Analytical Method:EPA 8015 Modified Preparation Method:EPA 3550 Sonication <br /> Motor Oil Range(C24-C36) 15.6 mg/kg 10 1 02/13/20 15:38 02/15/20 15:18 N2 <br /> TPH-DRO(C10-C28) ND mg/kg 10 1 02/13/20 15:38 02/15/20 15:18 <br /> Surrogates <br /> o-Terphenyl(S) 81 %. 30-146 1 02/13/20 15:38 02/15/20 15:18 84-15-1 <br /> n-Triacontane(S) 70 %. 30-144 1 02/13/20 15:38 02/15/20 15:18 638-68-6 <br /> Sample: SS-6-14 Lab ID: 10508446011 Collected: 02/10/20 13:35 Received: 02/13/20 10:50 Matrix: Solid <br /> Results reported on a"wet-weight'basis <br /> Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual <br /> 8015 GCS THC-Diesel Analytical Method:EPA 8015 Modified Preparation Method:EPA 3550 Sonication <br /> Motor Oil Range(C24-C36) 710 mg/kg 197 20 02/13/20 15:38 02/17/20 20:42 N2 <br /> TPH-DRO(C10-C28) 5330 mg/kg 197 20 02/13/20 15:38 02/17/20 20:42 <br /> Surrogates <br /> o-Terphenyl(S) 0 %. 30-146 20 02/13/20 15:38 02/17/20 20:42 84-15-1 S4 <br /> n-Triacontane(S) 0 %. 30-144 20 02/13/20 15:38 02/17/20 20:42 638-68-6 S4 <br /> Sample: SS-6-46 Lab ID: 10508446012 Collected: 02/10/20 14:00 Received: 02/13/20 10:50 Matrix: Solid <br /> Results reported on a "wet-weight'basis <br /> Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual <br /> 8015 GCS THC-Diesel Analytical Method:EPA 8015 Modified Preparation Method:EPA 3550 Sonication <br /> Motor Oil Range(C24-C36) 10.5 mg/kg 9.8 1 02/13/20 15:38 02/15/20 17:13 N2 <br /> TPH-DRO(C10-C28) 10.8 mg/kg 9.8 1 02/13/20 15:38 02/15/20 17:13 <br /> Surrogates <br /> o-Terphenyl(S) 84 %. 30-146 1 02/13/20 15:38 02/15/20 17:13 84-15-1 <br /> n-Triacontane(S) 63 %. 30-144 1 02/13/20 15:38 02/15/20 17:13 638-68-6 <br /> Sample: SS-7-17 Lab ID: 10508446013 Collected: 02/11/20 10:09 Received: 02/13/20 10:50 Matrix: Solid <br /> Results reported on a"wet-weight'basis <br /> Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual <br /> 8015 GCS THC-Diesel Analytical Method:EPA 8015 Modified Preparation Method:EPA 3550 Sonication <br /> Motor Oil Range(C24-C36) 613 mg/kg 480 50 02/13/20 15:38 03/01/20 00:25 N2 <br /> TPH-DRO(C10-C28) 8550 mg/kg 480 50 02/13/20 15:38 03/01/20 00:25 <br /> Surrogates <br /> o-Terphenyl(S) 0 %. 30-146 50 02/13/20 15:38 03/01/20 00:25 84-15-1 S4 <br /> n-Triacontane(S) 0 %. 30-144 50 02/13/20 15:38 03/01/20 00:25 638-68-6 S4 <br /> REPORT OF LABORATORY ANALYSIS <br /> This report shall not be reproduced,except in full, <br /> Date:03/20/2020 02:52 PM without the written consent of Pace Analytical Services,LLC. Page 11 of 39 <br />