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Foothill Landfill <br />Monitoring Implementation Plan <br /> <br /> <br /> <br />MIP Page 18 <br />The RWQCB requires the results of WDR storm water monitoring to be summarized in the <br />monitoring reports specified by the Order. If there is no discharge from the site during the <br />monitoring period, or the County did not obtain samples of the discharge, the County is <br />required to specify the reasons and circumstances in the monitoring report. <br />4.2 Sample Procedures <br />In order to provide effective sample management, San Joaquin County uses the following <br />sample management procedures that are derived from federal and state hazardous waste <br />regulations and guidance materials. Appendix F provides a summary of sampling procedures. <br />4.2.1 Sample Preservation and Storage <br />Sample preservation is dependent on the specific analyses that are to be performed. Each <br />sample is to be collected in sample containers provided by the laboratory. The required <br />analyses call for different preservation techniques. For example, the pH of the samples taken <br />for the Oil and Grease analysis must be lowered to less than 2 with sulfuric acid (H2SO4). For <br />some parameters, such as TSS, the only preservation technique required is refrigeration. The <br />laboratory provides the proper containers with the appropriate preservatives already added to <br />the containers. Measurement of pH may be field-tested; performed by the sampler, using a <br />calibrated pH meter or (if still at Baseline status, and never having reached Level 1 Status) <br />litmus paper. A summary of preservation techniques is included in Appendix B, including <br />Analytical methods, holding times, and annual and instantaneous NALs. <br />Sample storage is an integral part of the sample preservation. The samples are to be stored <br />until they are transported to the laboratory at a temperature of 4 degrees Celsius either in a <br />refrigerator or on ice in a cooler. A summary of storage temperatures is also included in <br />Appendix B. <br />4.2.2 Sample Labels <br />Each sample is labeled with labels provided by the laboratory and contains the following <br />information: <br />• Facility Name <br />• Sample Point as follows: “ST-2” <br />• Initials of Sampling Personnel <br />• Date and time of collection <br />• Preservative present in container (i.e. “Hydrochloric Acid” or “HCl”) <br />4.2.3 Sample Log / Sample Collection Information <br />General sampling information is recorded on the Chain of Custody at the time of sampling in <br />sufficient detail so that such information can be readily available. <br />• Facility Name <br />• Sample Point/Location (i.e. ST-2) <br />• Signature and Printed Name of Person Responsible for Sampling