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Client Sample Results Client: Union Pacific Railroad TestAmerica Job ID: 720-74752-1 Project/Site: UPRR-Stockton Client Sample ID: MR505 UPRRST160927 Lab Sample ID: 720-74752-1 Date Collected: 09/27/16 11:34 Matrix:Solid Date Received:09/28/16 09:05 Method: 8270C-Semivolatile Compounds by Gas Chromatography/Mass Spectrometry(GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 13 Phenol NO 3.3 0.27 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Bis(2-chloroethyl)ether NO 3.3 0.34 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 2-Chlorophenol NO 3.3 0.18 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 1,3-Dichlorobenzene NO 3.3 0.20 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 1,4-Dichlorobenzene NO 3.3 0.44 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Benzyl alcohol NO 8.4 0.26 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 1,2-Dichlorobenzene NO 3.3 0.23 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 2-Methylphenol NO 3.3 0.25 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Methylphenol,3&4 NO 3.3 0.47 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 N-Nitrosodi-n-propylamine NO 3.3 1.6 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Hexachloroethane NO 3.3 1.6 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Nitrobenzene NO 3.3 0.69 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Isophorone NO 3.3 0.23 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 2-Nitrophenol NO 3.3 1.6 mg/Kg 10/10/1610:18 10/15/1600:04 5 2,4-Dimethylphenol NO 3.3 1.3 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Bis(2-chloroethoxy)methane NO 8.4 0.27 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 2,4-Dichlorophenol NO 16 0.22 mg/Kg 10/10/1610:18 10/15/1600:04 5 1,2,4-Thchlorobenzene NO 3.3 0.34 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Naphthalene NO 3.3 0.24 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 4-Chloroaniline NO 8.4 0.22 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Hexachlorobutadiene NO 3.3 0.26 mg/Kg 10/10/1610:18 10/15/1600:04 5 4-Chloro-3-methylphenol NO 8.4 0.27 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 2-Methylnaphthalene 0.73 J 3.3 0.31 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Hexachlorocyclopentadiene NO 8.4 1.3 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 2,4,6-Trichlorophenol NO 8.4 0.48 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 2,4,5-T6chlorophenol NO 3.3 0.21 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 2-Chloronaphthalene NO 3.3 0.24 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 2-Nitroaniline NO 16 1.7 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Dimethyl phthalate NO 8.4 0.29 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Acenaphthylene NO 3.3 0.28 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 3-Nitroaniline NO 8.4 1.9 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Acenaphthene NO 3.3 0.19 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 2,4-Dinitrophenol NO 33 3.3 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 4-Nitrophenol NO 16 1.7 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Dibenzofuran NO 3.3 0.26 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 2,4-Dinitrotoluene NO 3.3 1.6 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 2,6-Dinitrotoluene NO 3.3 1.7 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Diethyl phthalate NO 8.4 0.23 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 4-Chlorophenyl phenyl ether NO 8.4 0.29 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Fluorene NO 3.3 0.20 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 4-Nitroaniline NO 16 1.6 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 2-Methyl-4,6-dinitrophenol NO 16 1.7 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 N-Nitrosodiphenylamine NO 3.3 0.19 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 4-Bromophenyl phenyl ether NO 8.4 0.25 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Hexachlorobenzene NO 3.3 1.6 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Pentachlorophenol NO 33 0.79 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Phenanthrene NO 3.3 0.23 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Anthracene NO 3.3 0.21 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Di-n-butyl phthalate NO 8.4 1.6 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 TestAmerica Pleasanton Page 6 of 27 10/17/2016