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Client Sample Results Client: Union Pacific Railroad TestAmerica Job ID: 720-74752-1 Project/Site: UPRR-Stockton Client Sample ID: MR505 UPRRST160927 Lab Sample ID: 720-74752-1 Date Collected:09/27/16 11:34 Matrix:Solid Date Received:09/28/16 09:05 Method:8270C-Semivolatile Compounds by Gas Chromatography/Mass Spectrometry(GC/MS)(Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed oil Fac Fluoranthene 0.91 J 3.3 0.36 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Pyrene 2.1 J 3.3 0.19 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Butyl benzyl phthalate ND 8.4 0.27 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 3,3'-Dichlorobenzidine ND 8.4 0.49 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Benzo[a]anthracene NO 16 0.89 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Bis(2-ethylhexyl)phthalate 7.0 J 16 0.33 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Chrysene ND 3.3 1.6 mg/Kg 10/10/1610:18 10/15/1600:04 5 Di-n-octyl phthalate ND 8.4 0.24 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Benzo[b]fluoranthene ND 3.3 0.47 mg/Kg 10/10/1610:18 10/15/1600:04 5 Benzo[a]pyrene ND 3.3 0.33 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Benzo[k]fluoranthene ND 3.3 0.69 mg/Kg 10/10/1610:18 10/15/1600:04 5 Indeno[1,2,3-cd]pyrene ND 3.3 0.64 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Benzo[g,h,i]perylene ND 3.3 0.98 mg/Kg 10/10/1610:18 10/15/1600:04 5 Benzoic acid N D 16 1.7 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Azobenzene ND 3.3 0.29 mg/Kg 10/10/1610:18 10/15/1600:04 5 Dibenz(a,h)anthracene ND 3.3 0.74 mg/Kg 10/10/16 10:18 10/15/16 00:04 5 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Nitrobenzene-d5 0 X 21-98 10/10/16 10:18 -1-01-1511600 04 5 2-Fluorobiphenyl 0 X 30-112 10/10/16 10:18 10/15/16 00:04 5 Terphenyl-d14 0 X 59-134 10/10/16 10:18 10/15/16 00:04 5 2-Fluorophenol 0 X 28-98 10/10/16 10:18 10/15/16 00:04 5 Phenol-d5 0 X 23-101 10/10/16 10:18 10/15/16 00:04 5 2,4,6-Tribromophenol 0 X 37-114 10/10/1610:18 10/15/1600:04 5 Method: 8015B-Diesel Range Organics(DRO)(GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Diesel Range Organics[C10-C28] 5900 99 mg/Kg - --i-0-/0711609-.39 10/07/16 21:54 100 Motor Oil Range Organics 12000 5000 mg/Kg 10/07/16 09:39 10/07/16 21:54 100 [C24-C36] Surrogate %Recovery Qualfer Limits Prepared Analyzed Dil Fac p-Terphenyl 0 X D 40-130 10/07/16 09:39 10/07/16 21:54 100 Method:6010B-Metals(ICP) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony 1.4 1.3 mg/Kg 09/30/16 12:36 10/04/16 22:29 4 Arsenic 3.1 2.7 mg/Kg 09/30/16 12:36 10/04/16 22:29 4 Barium 88 1.3 mg/Kg 09/30/1612:36 10/04/1622:29 4 Beryllium ND 0.27 mg/Kg 09/30/16 12:36 10/04/16 22:29 4 Cadmium ND 0.34 mg/Kg 09/30/1612:36 10/04/1622:29 4 Chromium 14 1.3 mg/Kg 09/30/16 12:36 10/04/16 22:29 4 Cobalt 1.8 0.54 mg/Kg 09/30/16 12:36 10/04/16 22:29 4 Copper 51 4.0 mg/Kg 09/30/16 12:36 10/04/16 22:29 4 Lead 10 1.3 mg/Kg 09/30/16 12:36 10/04/16 22:29 4 Molybdenum 77 1.3 mg/Kg 09/30/16 12:36 10/04/16 22:29 4 Nickel 7.9 1.3 mg/Kg 09/30/16 12:36 10/04/16 22:29 4 Selenium ND 2.7 mg/Kg 09/30/1612:36 10/04/1622:29 4 Silver ND 0.67 mg/Kg 09/30/1612:36 10/04/1622:29 4 Thallium ND 1.3 mg/Kg 09/30/1612:36 10/04/1622:29 4 Vanadium 8.1 1.3 mg/Kg 09/30/16 12:36 10/04/16 22:29 4 TestAmerica Pleasanton Page 7 of 27 10/17/2016