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QC Sample Results Client: Union Pacific Railroad TestAmerica Job ID: 720-74752-1 Project/Site: UPRR-Stockton Method: 8270C -Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) (Continued) Lab Sample ID: MB 720-210923/1-A Client Sample ID:Method Blank Matrix:Solid Prep Type:Total/NA Analysis Batch:211028 Prep Batch:210923 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Di-n-butyl phthalate ND 0.17 mg/Kg 10/10/1610:14 10/11/1623:35 1 Fluoranthene ND 0.067 mg/Kg 10/10/16 10:14 10/11/16 23:35 1 Pyrene ND 0.067 mg/Kg 10/10/16 10:14 10/11/16 23:35 1 Butyl benzyl phthalate ND 0.17 mg/Kg 10/10/16 10:14 10/11/16 23:35 1 • 3,3'-Dichlorobenzidine ND 0.17 mg/Kg 10/10/16 10:14 10/11/16 23:35 1 Benzo[a]anthracene ND 0.33 mg/Kg 10/10/16 10:14 10/11/16 23:35 1 Bis(2-ethylhexyl)phthalate ND 0.33 mg/Kg 10/10/16 10:14 10/11/16 23:35 1 Chrysene ND 0.067 mg/Kg 10/10/16 10:14 10/11/16 23:35 1 Di-n-octylphthalate ND 0.17 mg/Kg 10/10/1610:14 10/11/1623:35 1 Benzo[b]fluoranthene ND 0.067 mg/Kg 10/10/1610:14 10/11/1623:35 1 Benzo[a]pyrene ND 0.067 mg/Kg 10/10/1610:14 10/11/1623:35 1 Benzo[k]fluoranthene ND 0.067 mg/Kg 10/10/1610:14 10/11/1623:35 1 Indeno[1,2,3-cd]pyrene ND 0.067 mg/Kg 10/10/16 10:14 10/11/16 23:35 1 Benzo[g,h,i]perylene ND 0.067 mg/Kg 10/10/16 10:14 10/11/16 23:35 1 Benzoic acid ND 0.33 mg/Kg 10/10/1610:14 10/11/1623:35 1 Azobenzene ND 0.067 mg/Kg 10/10/16 10:14 10/11/16 23:35 1 Dibenz(a,h)anthrace ne ND 0.067 mg/Kg 10/10/16 10:14 10/11/16 23:35 1 MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Nitrobenzene-d5 80 21-98 10110116 10:14 10111116 23:35 1 2-Fluorobiphenyl 94 30-112 10110116 10:14 10111116 23:35 1 Terphenyl-d14 111 59-134 10110116 10:14 10111116 23:35 1 2-Fluorophenol 76 28-98 10110116 10:14 10111116 23:35 1 Phenol-d5 72 23-101 10110116 10:14 10111116 23:35 1 2,4,6-Tribromophenol 82 37-114 10110116 10:14 10111116 23:35 1 Lab Sample ID: LCS 720-210923/2-A Client Sample ID:Lab Control Sample Matrix:Solid Prep Type:Total/NA Analysis Batch:211028 Prep Batch:210923 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Phenol 1.33 1.00 mg/Kg 75 48-115 Bis(2-chloroethyl)ether 1.33 0.941 mg/Kg 71 45-115 2-Chlorophenol 1.33 1.01 mg/Kg 76 48-115 1,3-Dichlorobenzene 1.33 0.960 mg/Kg 72 41-115 1,4-Dichlorobenzene 1.33 0.950 mg/Kg 71 40-115 Benzyl alcohol 1.33 0.988 mg/Kg 74 51-115 1,2-Dichlorobenzene 1.33 0.988 mg/Kg 74 44-115 2-Methylphenol 1.33 0.977 mg/Kg 73 54-115 Methylphenol,3&4 1.33 1.11 mg/Kg 83 42-115 N-Nitrosodi-n-propylamine 1.33 1.03 mg/Kg 77 46-115 Hexachloroethane 1.33 0.946 mg/Kg 71 44-115 Nitrobenzene 1.33 1.04 mg/Kg 78 48-115 Isophorone 1.33 1.03 mg/Kg 77 54-115 2-Nitrophenol 1.33 0.944 mg/Kg 71 48-115 2,4-Dimethylphenol 1.33 1.19 mg/Kg 89 52-115 Bis(2-chloroethoxy)methane 1.33 1.04 mg/Kg 78 46-115 TestAmerica Pleasanton Page 11 of 27 10/17/2016