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QC Sample Results Client: Union Pacific Railroad TestAmerica Job ID: 720-74752-1 Project/Site: UPRR-Stockton Method: 8270C -Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) (Continued) Lab Sample ID:LCS 720-210923/2-A Client Sample ID: Lab Control Sample Matrix:Solid Prep Type:Total/NA Analysis Batch:211028 Prep Batch:210923 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits 2,4-Dichlorophenol 1.33 1.11 mg/Kg 83 49-100 1,2,4-Trichlorobenzene 1.33 1.01 mg/Kg 76 47-115 Naphthalene 1.33 1.04 mg/Kg 78 44-115 4-Chloroaniline 1.33 0.943 mg/Kg 71 30-115 • Hexachlorobutadiene 1.33 1.00 mg/Kg 75 44-115 4-Chloro-3-methylphenol 1.33 1.14 mg/Kg 86 58-115 2-Methylnaphthalene 1.33 1.09 mg/Kg 82 49-115 Hexachlorocyclopentadiene 1.33 0.955 mg/Kg 72 42-132 2,4,6-Trichlorophenol 1.33 1.14 mg/Kg 86 45-115 2,4,5-Trichlorophenol 1.33 1.13 mg/Kg 85 48-115 2-Chloronaphthalene 1.33 1.06 mg/Kg 80 52-115 2-Nitroaniline 1.33 1.06 mg/Kg 79 54-115 Dimethyl phthalate 1.33 1.17 mg/Kg 88 64-119 Acenaphthylene 1.33 1.09 mg/Kg 82 61-129 3-Nitroaniline 1.33 0.982 mg/Kg 74 50-115 Acenaphthene 1.33 1.14 mg/Kg 86 50-115 2,4-Dinitrophenol 2.67 2.02 mg/Kg 76 15-115 4-Nitrophenol 2.67 2.41 mg/Kg 90 54-125 Dibenzofuran 1.33 1.11 mg/Kg 83 55-115 2,4-Dinitrotoluene 1.33 1.12 mg/Kg 84 57-115 2,6-Dinitrotoluene 1.33 1.08 mg/Kg 81 54-119 Diethyl phthalate 1.33 1.20 mg/Kg 90 49-117 4-Chlorophenyl phenyl ether 1.33 1.15 mg/Kg 86 57-115 Fluorene 1.33 1.10 mg/Kg 83 54-115 4-Nitroaniline 1.33 1.19 mg/Kg 89 59-115 2-Methyl 4,6-d initrophenol 2.67 2.16 mg/Kg 81 39-115 N-Nitrosodiphenylamine 1.33 1.11 mg/Kg 83 56-115 4-Bromophenyl phenyl ether 1.33 1.16 mg/Kg 87 53-115 Hexachlorobenzene 1.33 1.15 mg/Kg 87 55-115 Pentachlorophenol 2.67 2.31 mg/Kg 87 35-115 Phenanthrene 1.33 1.13 mg/Kg 85 54-115 Anthracene 1.33 1.18 mg/Kg 88 55-115 Di-n-butyl phthalate 1.33 1.23 mg/Kg 92 55-115 Fluoranthene 1.33 1.23 mg/Kg 92 52-130 Pyrene 1.33 1.24 mg/Kg 93 48-115 Butyl benzyl phthalate 1.33 1.23 mg/Kg 93 53-115 3,3'-Dichlorobenzidine 1.33 1.06 mg/Kg 79 42-115 Benzo[a]anthracene 1.33 1.17 mg/Kg 88 55-115 Bis(2-ethylhexyl)phthalate 1.33 1.29 mg/Kg 97 53-115 Chrysene 1.33 1.17 mg/Kg 88 58-115 Di-n-octyl phthalate 1.33 1.24 mg/Kg 93 53-115 Benzo[b]fluoranthene 1.33 1.25 mg/Kg 94 50-119 Benzo[a]pyrene 1.33 1.20 mg/Kg 90 57-122 Benzo[k]fluoranthene 1.33 1.17 mg/Kg 88 55-120 Indeno[1,2,3-cd]pyrene 1.33 1.16 mg/Kg 87 56-115 Benzo[g,h,i]perylene 1.33 1.07 mg/Kg 80 56-115 Benzoic acid 1.33 0.918 mg/Kg 69 10-115 TestAmerica Pleasanton Page 12 of 27 10/17/2016