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Pace Analytical Services, Inc. <br />_ aceAnalytical 2795 Second Street- Suite 300 <br />Davis, CA 95618 <br />-pacelabs.com (530) 297-4800 <br />QUALITY CONTROL DATA <br />Project: Valley Pacific Fresno Ave. <br />Pace Project No.: 1263778 <br />MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 304957 <br />1263477008 <br />Parameter Units Result <br />MS <br />Spike <br />Conc. <br />MSD <br />Spike <br />Conc. <br />304958 <br />MS <br />Result <br />MSD <br />Result <br />MS <br />% Rec <br />MSD <br />% Rec <br />% Rec <br />Limits <br />Max <br />RPD RPD Qual <br />1,1,1,2 -Tetrachloroethane <br />ug/kg <br /><0.097 <br />39.4 <br />39 <br />34.4 <br />35.0 <br />87 <br />90 <br />33-133 <br />2 <br />25 <br />1,1,1 -Trichloroethane <br />ug/kg <br /><0.054 <br />39.4 <br />39 <br />36.0 <br />35.8 <br />91 <br />92 <br />54-126 <br />0 <br />25 <br />1,1,2,2 -Tetrachloroethane <br />ug/kg <br /><0.12 <br />39.4 <br />39 <br />35.2 <br />34.6 <br />89 <br />89 <br />30-145 <br />2 <br />25 <br />1,1,2 -Trichloroethane <br />ug/kg <br /><0.13 <br />39.4 <br />39 <br />36.7 <br />36.1 <br />93 <br />93 <br />30-134 <br />2 <br />25 <br />1,1-Dichloroethane <br />ug/kg <br /><0.071 <br />39.4 <br />39 <br />37.4 <br />35.5 <br />95 <br />91 <br />51-125 <br />5 <br />25 <br />1,1-Dichloroethene <br />ug/kg <br /><0.097 <br />39.4 <br />39 <br />37.5 <br />36.6 <br />95 <br />94 <br />60-125 <br />2 <br />25 <br />1,1-Dichloropropene <br />ug/kg <br /><0.087 <br />39.4 <br />39 <br />36.9 <br />35.1 <br />94 <br />90 <br />54-125 <br />5 <br />25 <br />1,2,3-TrichI oro benzene <br />ug/kg <br /><0.14 <br />39.4 <br />39 <br />33.2 <br />30.9 <br />84 <br />79 <br />30-125 <br />7 <br />25 <br />1,2,3-Trichloropropane <br />ug/kg <br /><0.19 <br />39.4 <br />39 <br />36.8 <br />36.3 <br />93 <br />93 <br />32-125 <br />1 <br />25 <br />1,2,4-Trichlorobenzene <br />ug/kg <br /><0.13 <br />39.4 <br />39 <br />32.1 <br />30.0 <br />81 <br />77 <br />30-125 <br />7 <br />25 <br />1,2,4 -Tri methyl benzene <br />ug/kg <br />0.24J <br />39.4 <br />39 <br />35.1 <br />34.1 <br />88 <br />87 <br />30-131 <br />3 <br />25 <br />1,2-Dibromo-3- <br />ug/kg <br /><0.81 <br />98.6 <br />97.5 <br />85.3 <br />85.3 <br />87 <br />87 <br />30-142 <br />0 <br />25 <br />chloropropane <br />1,2-Dibromoethane (EDB) <br />ug/kg <br /><0.096 <br />39.4 <br />39 <br />36.7 <br />36.1 <br />93 <br />93 <br />46-125 <br />2 <br />25 <br />1,2 -Dichlorobenzene <br />ug/kg <br /><0.15 <br />39.4 <br />39 <br />35.5 <br />33.8 <br />90 <br />87 <br />30-125 <br />5 <br />25 <br />1,2-Dichloroethane <br />ug/kg <br /><0.071 <br />39.4 <br />39 <br />37.3 <br />36.2 <br />95 <br />93 <br />46-125 <br />3 <br />25 <br />1,2-Dichloropropane <br />ug/kg <br /><2.4 <br />39.4 <br />39 <br />37.4 <br />36.7 <br />95 <br />94 <br />41-125 <br />2 <br />25 <br />1,3,5 -Tri methyl benzene <br />ug/kg <br /><0.076 <br />39.4 <br />39 <br />35.6 <br />34.8 <br />90 <br />89 <br />30-132 <br />2 <br />25 <br />1,3 -Dichlorobenzene <br />ug/kg <br /><0.071 <br />39.4 <br />39 <br />34.3 <br />32.7 <br />87 <br />84 <br />30-125 <br />5 <br />25 <br />1,3-Dichloropropane <br />ug/kg <br /><0.072 <br />39.4 <br />39 <br />38.3 <br />37.1 <br />97 <br />95 <br />32-125 <br />3 <br />25 <br />1,4 -Dichlorobenzene <br />ug/kg <br /><0.11 <br />39.4 <br />39 <br />34.5 <br />32.6 <br />88 <br />84 <br />30-125 <br />6 <br />25 <br />2,2-Dichloropropane <br />ug/kg <br /><0.16 <br />39.4 <br />39 <br />37.0 <br />35.9 <br />94 <br />92 <br />52-127 <br />3 <br />25 <br />2-Chlorotoluene <br />ug/kg <br /><0.15 <br />39.4 <br />39 <br />35.2 <br />34.1 <br />89 <br />87 <br />30-125 <br />3 <br />25 <br />4-Chlorotoluene <br />ug/kg <br /><0.14 <br />39.4 <br />39 <br />34.4 <br />33.3 <br />87 <br />86 <br />30-125 <br />3 <br />25 <br />Benzene <br />ug/kg <br />0.24J <br />39.4 <br />39 <br />37.1 <br />36.0 <br />94 <br />92 <br />56-125 <br />3 <br />25 <br />Bromobenzene <br />ug/kg <br /><0.076 <br />39.4 <br />39 <br />34.8 <br />33.7 <br />88 <br />86 <br />30-125 <br />3 <br />25 <br />Bromochloromethane <br />ug/kg <br /><0.17 <br />39.4 <br />39 <br />36.4 <br />35.4 <br />92 <br />91 <br />45-125 <br />3 <br />25 <br />Bromodichloromethane <br />ug/kg <br /><0.097 <br />39.4 <br />39 <br />31.0 <br />31.3 <br />79 <br />80 <br />31-132 <br />1 <br />25 <br />Bromoform <br />ug/kg <br /><0.35 <br />39.4 <br />39 <br />25.2 <br />25.5 <br />64 <br />65 <br />30-125 <br />1 <br />25 <br />Bromomethane <br />ug/kg <br /><0.29 <br />39.4 <br />39 <br />27.0 <br />25.5 <br />68 <br />65 <br />30-139 <br />6 <br />25 <br />Carbon tetrachloride <br />ug/kg <br /><0.11 <br />39.4 <br />39 <br />31.3 <br />32.6 <br />79 <br />84 <br />49-130 <br />4 <br />25 <br />Chlorobenzene <br />ug/kg <br /><0.11 <br />39.4 <br />39 <br />35.3 <br />34.8 <br />89 <br />89 <br />33-125 <br />1 <br />25 <br />Chloroethane <br />ug/kg <br /><0.18 <br />39.4 <br />39 <br />34.4 <br />34.2 <br />87 <br />88 <br />30-150 <br />1 <br />25 <br />Chloroform <br />ug/kg <br /><0.091 <br />39.4 <br />39 <br />38.9 <br />37.6 <br />99 <br />96 <br />46-125 <br />3 <br />25 <br />Chloromethane <br />ug/kg <br /><0.15 <br />39.4 <br />39 <br />30.4 <br />29.4 <br />77 <br />75 <br />45-125 <br />3 <br />25 <br />cis-1,2-Dichloroethene <br />ug/kg <br /><0.097 <br />39.4 <br />39 <br />36.0 <br />35.0 <br />91 <br />90 <br />50-125 <br />3 <br />25 <br />cis-1,3-Dichloropropene <br />ug/kg <br /><0.083 <br />39.4 <br />39 <br />31.7 <br />31.0 <br />80 <br />80 <br />35-126 <br />2 <br />25 <br />Dibromochloromethane <br />ug/kg <br /><0.061 <br />39.4 <br />39 <br />28.9 <br />29.3 <br />73 <br />75 <br />30-130 <br />1 <br />25 <br />Dibromomethane <br />ug/kg <br /><0.13 <br />39.4 <br />39 <br />36.4 <br />34.8 <br />92 <br />89 <br />36-127 <br />4 <br />25 <br />Dichlorodifluoromethane <br />ug/kg <br /><0.19 <br />39.4 <br />39 <br />22.7 <br />22.3 <br />58 <br />57 <br />44-125 <br />2 <br />25 <br />Ethylbenzene <br />ug/kg <br />0.191 <br />39.4 <br />39 <br />36.6 <br />36.0 <br />92 <br />92 <br />45-125 <br />2 <br />25 <br />Hexachloro-1,3-butadiene <br />ug/kg <br /><0.13 <br />39.4 <br />39 <br />27.1 <br />24.1 <br />69 <br />62 <br />30-125 <br />11 <br />25 <br />Isopropylbenzene (Cumene) <br />ug/kg <br /><0.11 <br />39.4 <br />39 <br />36.1 <br />35.3 <br />92 <br />90 <br />35-128 <br />2 <br />25 <br />m&p-Xylene <br />ug/kg <br />0.62J <br />78.9 <br />78 <br />72.3 <br />70.5 <br />91 <br />90 <br />40-125 <br />2 <br />25 <br />Methylene Chloride <br />ug/kg <br /><0.25 <br />39.4 <br />39 <br />38.1 <br />36.1 <br />97 <br />92 <br />42-125 <br />5 <br />25 <br />n-Butylbenzene <br />ug/kg <br /><0.15 <br />39.4 <br />39 <br />34.7 <br />32.3 <br />88 <br />83 <br />30-127 <br />7 <br />25 <br />Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result <br />REPORT OF LABORATORY ANALYSIS <br />This report shall not be reproduced, except in full, <br />Date: 04/13/2016 04:40 PM without the written consent of Pace Analytical Services, Inc.. 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