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Alpha Analytical, Inc. <br /> 255 Glendale Ave. •Suite 21 •Sparks,Nevada 89431-5778 <br /> (775)355-1044• (775)355-0406 FAX• 1-800-283-1183 <br /> Work Order: <br /> 20p,-06 QC Summary Report 06041427 <br /> vlethod Blank Type MBLK Test Code: EPA Method SW8015B1DHS LUFT Manual <br /> =ile ID: C:IHPCHEM1MS101DATA1060417106041706.D Batch ID:MS10S4496B Analysis Date: 04/17/2006 09:55 <br /> 'ample ID: MBLK MS10S4496B Units: pg/Kg Run ID:MSD_10 060417A Prep Date: 04/17/2006 <br /> analyte Result PQL SpkVal SpkRefVal %REC LowUmit HighLimit RPDRefVal %RPD(Limit) Qual <br /> .PH-P(GRO) ND 1000 <br /> 'urr: 1,2-Dichloroethane-d4 164 200 82 68 119 <br /> 'urr:Toluene-d8 164 200 82 84 116 S54 <br /> �urr:4-Bromofluorobenzene 194 200 97 72 118 <br /> ,aborate y Control Spike Type LCS Test Code: EPA Method SW8015B1DHS LUFT Manual <br /> :ile ID: C:IHPCHEM1MS101DATA1060417106041710.D Batch ID:MS10S4496B Analysis Date: 0411712006 11:20 <br /> 'ample ID: GLCS MS10S4496B Units: pg/Kg Run 0:MSD_10_060417A Prep Date: 04/17/2006 <br /> ,nalyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qual <br /> PH-P(GRO) 19300 2000 16000 121 60 153 <br /> 'urr: 1,2-Dichloroethane-d4 323 400 81 68 119 <br /> urr:Toluene-d8 342 400 86 84 116 <br /> urr:4-Bromofluorobenzene 387 400 97 72 118 <br /> ample Matrix Spike Type MS Test Code: EPA Method SW8015B1DHS LUFT Manual <br /> Ile ID:C:IHPCHEM1MS10IDATA1060417106041711.D Batch ID:MS10S4496B Analysis Date: 04/17/2046 11:41 <br /> ample ID: 06041427-11AGS Units: pg/Kg Run ID:MSD_10_060417A Prep Date: 04/17/2006 <br /> nalyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qual <br /> PH-P(GRO) 16000 2000 16000 0 100 8 177 <br /> urr: 1,2-Dichloroethane-d4 365 400 91 68 119 <br /> urr:Toluene-d8 399 400 99.8 84 116 <br /> urr:4-Bromofluorobenzene 378 400 95 72 118 <br /> Matrix Spike Duplicate Type MSD Test Code: EPA Method SW8015B1DHS LUFT Manual <br /> ir9W. C:IHPCHEM1MS101DATA1060417106041712.D Batch ID:MSlDS4496B Analysis Date: 04/17/2006 12:02 <br /> ample ID: 06041427-11AGSO Units:pg/Kg Run 1D:MSD_10_060417A Prep Date: 04/1712006 <br /> nalyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qual <br /> PH-P(GRO) 15400 2000 16000 0 96 8 177 16000 4.1(45) <br /> urr: 1,2-Dichloroethane-d4 385 400 96 68 119 <br /> urr:Toluene-d8 402 400 101 84 116 <br /> urr:4-Bromofluorobenzene 384 400 96 72 118 <br /> omments: <br /> alculations are based off of raw(non-rounded)data.However,for reporting purposes,all QC data is rounded to three significant figures.Therefore,hand calculated <br /> flues may differ slightly. <br /> 34=Surrogate recovery was below laboratory acceptance limits- <br /> -ported in micrograms per kilogram,per client request. <br /> • <br />