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Alpha Analytical, Inc. <br /> 255 Glendale Ave. •Suite 21 • Sparks,Nevada 89431-5778 <br /> (775)355-1044• (775)355-0405 FAX• 1-800-283-1183 <br /> Work <br /> z,-o6 QC Summary Report fl6o4o42�`: <br /> Method Blank Type MBLK Test Code: EPA Method SW8260B <br /> :ile ID: C:IHPCHEM1MS101DATA1060417106041706.D Batch ID:MSlOS4496A Analysis Date: 04/1712006 09:55 <br /> ;'ample ID: MBLK MS10S4496A Units: pg/Kg Run ID:MSD_10_060417A Prep Date: 04/17/2006 <br /> analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVa[ %RPD(Limit) Qual <br /> "ertiary Butyl Alcohol(TBA) ND 500 <br /> Aethyl tert-butyl ether(MTBE) ND 5 <br /> )i-isopropyl Ether(DIPS) ND 20 <br /> :thyl Tertiary Butyl Ether(ETRE) ND 20 <br /> ,2-Dichloroethane ND 20 <br /> lenzene ND 5 <br /> "ertiary Amyl Methyl Ether(TAME) ND 20 <br /> oluene ND 5 <br /> ,2-Dibromoethane(EDB) ND 40 <br /> :thylbenzene ND 5 <br /> 1,p-Xylene ND 5 <br /> -Xylene ND 5 <br /> ,urr: 1,2-Dichloroethane-d4 164 200 82 68 119 <br /> -urr:Toluene-d8 164 200 82 84 116 S54 <br /> •urr:4-Bromofluorobenzene 194 200 97 72 118 <br /> ,aboratory Control Spike Type LCS Test Code: EPA Method SW8260B <br /> 'ile ID: C:IHPCHEMIMS101DATA1060417106041707.D Batch ID: MSIOS4496A Analysis Date: 0411 712006 10:16 <br /> ample ID: LCS MSlOS4496A Units: pg/Kg Run ID:MSD_10_060417A Prep Date: 04117/2006 <br /> nalyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qual <br /> enzene 349 10 400 87 58 147 <br /> oluene 385 10 400 96 58 148 <br /> thylbenzene 424 10 400 106 59 151 <br /> Dene 433 10 400 108 60 155 <br /> e 416 10 400 104 62 155 <br /> u 1,2-Dichloroethane-d4 346 400 86 68 119 <br /> urr:Toluene-d8 387 400 97 84 116 <br /> urr:4-Bromofluorobenzene 399 400 99.7 72 118 <br /> ample Matrix Spike Type MS Test Code: EPA Method SW8260B <br /> He ID: C:IHPCHEMIMSIOIDATAI060417106041708.D Batch ID:MSlOS4496A Analysis Date: 041171200610:37 <br /> ample ID: 06041427-11AMS Units: pg/Kg Run ID:MSD_10_060417A Prep Date: 04/17/2006 <br /> nalyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qual <br /> enzene 333 10 400 0 83 30 151 <br /> 31uene 373 10 400 0 93 25 159 <br /> thylbenzene 426 10 400 0 107 27 161 <br /> ,p-Xylene 453 10 400 22.24 108 22 170 <br /> Xylene 420 10 400 7"45 103 22 171 <br /> urr: 1,2-Dichloroethane-d4 345 400 86 68 119 <br /> urr:Toluene-d8 383 400 96 84 116 <br /> jrr:4-Bromofluorobenzene 397 400 99 72 118 <br /> ample Matrix Spike Duplicate Type MSD Test Code: EPA Method SW8260B <br /> ale ID: C:IHPCHEMIMSIOIDATAI060417106041709.0 Batch ID: MS10S"96A Analysis Date: 041171200610:59 <br /> ample ID: 06041427-11AMSD Units: jig/Kg Run ID:MSa_10_060417A Prep Date: 04/17/2006 <br /> iaiyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qual <br /> ;nzene 319 10 400 0 80 30 151 332.7 4.2(37) <br /> )luene 368 10 400 0 92 25 159 372.6 1.4(40) <br /> :hylbenzene 405 10 400 0 101 27 161 426 5.0(39) <br /> ,p-Xylene 442 10 400 22.24 105 22 170 453"4 2.6(40) <br /> Xylene 398 10 400 7.45 98 22 171 420.2 5.5(41) <br /> irr: 1,2-Dichloroethane-d4 356 400 89 68 119 <br /> jrr:Toluene-d8 393 400 98 84 116 <br /> irr:4-Bromofluorobenzene 398 400 99.6 72 118 <br /> 0 <br />