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COLUMBIA ANALYTICAL SERVICES,INC <br /> Analytical Report <br /> Client E;MCON Service Request S9900683 <br /> Protect Apache Plastics/22640-100 001 Date Collected 2/22/99 <br /> Sample Matrix Water Date Received 3/2/99 <br /> BTEX,MTBE and TPH as Gasoline <br /> Sample Name 11P-2(76) Units ug/L(ppb) <br /> Lab Code S9900683-017 Basis NA <br /> Test Notes <br /> i <br /> i <br /> Prep Analysts Dilution Date Date Result <br /> Analyte Method Method MRL Factor Extracted Analyzed Result Notes <br /> TPH as Gasoline EPA 5030 CA/LUFT 50 1 NA 3/7/99 ND <br /> Benzene EPA 5030 8020 05 1 NA 3/7/99 ND <br /> i <br /> Toluene EPA 5030 8020 05 1 NA 3/7/99 ND <br /> Ethylbenzene EPA 5030 8020 05 l NA 3/7/99 ND <br /> Xylenes,Total EPA 5030 8020 05 1 NA 3/7/99 ND <br /> Methyl ler!-Butyl Ether EPA 5030 8020 3 1 NA 3/7/99 ND <br /> • <br /> iszzrozose7p <br /> Page 39 <br />