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COLUMBIA ANALYTICAL SERVICES,INC <br /> Analytical Report <br /> 49 Client CMCON Service Request 59900683 <br /> Project Apache Plastics/22640-100 001 Date Collected 2/22/99 <br /> Sample Matrix Wdwr Date Received 312199 <br /> BTEX,NnBE and TPH as Gasoline <br /> Sample Name 1-IP-2(90) Units ug/L(ppb) <br /> Lab Code 59900683-01 R <br /> Test Notes Bests NA <br /> Prcp Analvus Dilution Date Date Result <br /> Analyte Method Method MRL Factor Extracted Analyzed Result Notes <br /> TPH as Gasoline EPA 5030 CA/1-UFT 50 1 NA 3/7/99 ND <br /> Benzene EPA 5030 8020 05 1 NA 3/7/99 ND <br /> Toluene EPA 5030 8020 05 1 NA 3/7/99 ND <br /> Ethylbenzene EPA 5030 8020 0 5 1 NA 3/7/99 ND <br /> Xylenes,Total EPA 5030 8020 05 1 NA 3/7/99 ND <br /> Methyl Cert-Butyl Ether EPA X030 8020 3 l NA 3/7/99 ND <br /> isxvoxassap <br /> Page 40 <br />