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COLUMBIA ANALYTICAL SERVICES, INC <br /> Analytical Report <br /> Client EMCON Service Request 59900683 <br /> Protect Apache Plastrc,s/22640-100 001 Date Colkcted 2/23/99 <br /> Samplc Matrix Soil Date Received 3/2/99 <br /> BTEX,MTBE and TPH as Gasoline <br /> Soluble Tlire,,hold Limit Concentration(STLC) <br /> Sample Name R-1(82) Units ug/L(ppb) <br /> Ldb Code 53900683-008 Basis NA <br /> Test Notes <br /> Prep Analysis STLC Dilution Date Date Result <br /> Anal)te Method Method MRL Luruts' Factor Extracted Analyzed Result Notes <br /> TPH as Gasoline EPA 5030 CA/LUFT 500 1 3/6-8/99 3/9/99 3700 <br /> Benzene EPA 5030 8020 5 1 3/6-8/99 3/9/99 150 <br /> Toluene EPA 5030 8020 5 1 3/6-8/99 3/9/99 620 <br /> Ethylbenzene EPA 5030 8020 5 1 3/6-8/99 3/9/99 70 <br /> Xylenes,Total EPA 5030 8020 5 1 3/6-8199 3/9/99 460 <br /> Methyl Cert-Butyl Ether EPA 5030 8020 30 1 3/6-8/99 3/9/99 ND <br /> 0 15221020597p <br /> Page 45 <br />