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COLUMBIA ANALYTICAL SERVICES,INC <br /> Analytical Report <br /> Client EMCON Service Request 59900683 <br /> Protect Apache Plastics/22640-100 001 Date Collected 2/22/99 <br /> Sample Matrix Soil Date Received 3/2/99 <br /> BTFX,MTBE~and TPH as Gasoline <br /> Soluble Threshold Limit Concentration(STLC) <br /> Sample Name B-2(102) Units ug/L.(ppb) <br /> Lab Code S9900683-012 Basis NA <br /> Test Notes <br /> Prep Analysis STLC Dilution Date Date Result <br /> Analyte Method Method MRL Limits' Factor Extracted Analyzed Result Notes <br /> TPH as Gasoline EPA 5030 CA/LU17 500 1 3/6-8/99 3/11/99 ND <br /> Benzene EPA 5030 8020 5 1 3/6-8/99 3/11/99 ND <br /> Toluene EPA 5030 8020 5 1 3/6-8/99 3/11/99 ND <br /> Ethylbenzene EPA 5030 8020 5 1 3/6-8/99 3/11/99 ND <br /> Xylenes,Total EPA 5030 8020 5 1 3/6-8/99 3/11/99 ND <br /> Methyl Cert-Butyl Ether EPA 5030 8020 30 1 3/6-8/99 3/11199 ND <br /> ]S221020597p <br /> Page 46 <br />