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COLUMBIA ANALYTICAL SERVICES, INC <br /> Analytical Report <br /> Client EMC.ON Service Request 59900683 <br /> Project Apache Plastic,/22640-100 001 Date Collected 2/23/99 <br /> Sample Mati ix Soil Date Received* 3/2/99 <br /> Fuel Oxygenates <br /> Soluble Threshold Limit Concentration(STLC) <br /> Sample Nan1e B-1(82} Units uglL,(ppb) <br /> Lab Code 59900683-008 Basis NA <br /> Test Notes <br /> P1 ep Analysis STLC Dilution Date Date Result <br /> Analyte Method Method MRL Limns* Factor Extracted Analyzed Result Notes <br /> tert-Butyl Alcohol NONE 8260 500 - 1 NA 3/10/99 ND <br /> Methyl tert-But)7l Ether NONE 8260 5 - 1 NA 3/10/99 ND <br /> Diisopropyl Ether NONE 8260 50 - 1 NA 3/10199 ND <br /> Ethyl tent-Butyl Ether NONE 8260 50 - 1 NA 3/10/99 ND <br /> Cert-Amyl Methyl Ether NONE 8260 50 - 1 NA 3/10199 ND <br /> Ethanol NONE 8260 5000 - ] NA 3/10/99 ND <br /> I <br /> t I-WO2 P97p <br /> Page 21 <br />