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COLUMBIA ANALYTICAL SERVICES, INC <br /> Analytical Report <br /> Client EMCON Service Request 59900683 <br /> Protect Apache Plastics/22690-100 001 Date Collected 2/22/99 <br /> Sample Mati to Soil Date Received 3/2/99 <br /> Fuel Oxygenates <br /> Soluble I Itreshold Limit Concentration(STLC) <br /> Sample Name B-2(102) Units ug/L(ppb) <br /> Lab Code 59900683-012 Basis NA <br /> Test Notes <br /> Pzel) Analysis STLC Dilution Date Date Result <br /> Analyte Method Method MRL Limits" Factor Extracted Analyzed Result Notes <br /> tent-Butyl Alcohol NONE 8260 500 - 1 NA 3/10/99 ND <br /> Methyl tent-Butyl Ethel NONE 8260 5 - l NA 3/10/99 ND <br /> Ditsopropyl Ether NONE 8260 50 - 3 NA 3/10/99 ND <br /> Ethyl tent-Butyl Ether NONE 8260 50 - 1 NA 3/10199 ND <br /> tert-Amyl Methyl Ether NONE 8260 50 - 1 NA 3/10/99 ND <br /> Ethanol NONE 8260 5000 - 1 NA 3/10/99 ND <br /> I <br /> 1S44/021197P <br /> Page 22 <br />