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COLUMBIA ANALYTICAL SERVICES,INC <br /> Analytical Report <br /> Client EMCON Service Request S9900683 <br /> Protect Ahathe Plastics/22640-100 001 Date Collected 2/23/99 <br /> Sample Matrix Soil Date Received 3/2/99 <br /> BTEX,MTBE and TPH as Gasoline <br /> Sample Name B-1(74) Units mg/Kg(ppm) <br /> Ldb Code S990069�-007 Basis Wet <br /> Test Notes <br /> Prep Analysis Dilution Date Date Result <br /> Analyte Method Method MRL Factor Extracted Analyzed Result Notes <br /> TPH as Gasoline EPA 5030 CA/LUFT 1 100 3/4/99 3/7/99 1000 <br /> Benzene EPA 5030 8020 0 005 100 3/4/99 3/7199 10 <br /> Toluene EPA 5030 8020 0 005 100 3/4/99 3/7199 68 <br /> Ethylbenzene EPA 5030 8020 0 005 100 3/4/99 3/7/99 22 <br /> Xylenes,Total EPA 5030 8020 0 005 100 3/4199 3/7/99 120 <br /> Methyl tert-Butyl Ether EPA 5030 8020 005 100 3/4/99 3/7/99 <5 C1 <br /> Cl. The MRL,was elevated due to high analyte concentration requiring sample dilution <br /> IS22/020597p <br /> Page 27 <br />