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COLUMBIA ANALYTICAL SERVICES,INC <br /> Analytical Report <br /> Client EMCON Service,Requf-st S9900683 <br /> Protect Apadhe Phs,,w.,/22640-100 001 Date Collected 2/23/99 <br /> Sample Matrix Soil Date Received 3/2/99 <br /> i <br /> BTEX,MTBE and TPH as Gasoline <br /> i <br /> Sample Name B-3(82) Unit, mg/Kg(ppm) <br /> Lab Code 59900683-008 Basis Wet <br /> Test Notes <br /> Prep Analysis Dilution Date Date Result <br /> Analyte Method Method MILL Factor Extracted Analyzed Result Notes <br /> TPH as Ga%ohne EPA 5030 CA/LUI'T 1 50 3/4/99 3/7/99 490 <br /> Benzene EPA 5030 8020 0 005 50 3/4/99 3/7/99 49 <br /> Toluene EPA 5030 8020 0 005 50 3/4/99 3/7199 33 <br /> Ethylbenzene EPA 5030 8020 0 005 50 3/4/99 3/7/99 11 <br /> Xylenes,Total EPA-)030 8020 0 005 50 3/4/99 3/7/99 72 <br /> Methyl tert-Butyl Ether EPA 5030 8020 005 50 3/4/99 3/7199 <2 5 C1 <br /> C1 The MRI,tva,elevated due to high analyte concentration requiring sample dilution <br /> I g22/020Wp <br /> Page 28 <br />