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COLUMBIA ANALYTICAL SERVICES,INC <br /> Analytical Report <br /> Client EMCON Service Request S9900683 <br /> Protect Apache Plastics/22640-100 001 Date Collected 2/22/99 <br /> Sample MAtrix Soil Date Received 3/2/99 <br /> BTEX,MTBE and TPH as Gasoline <br /> Sample Name B-2(82) Units mg/Kg(ppm) <br /> Lab Code 59900683-010 Basis Wet <br /> Test Notes <br /> Prep AnAlysis Dilution Date Date Result <br /> Analyte Method Method MRL Factor Extracted Analyzed Result Notes <br /> TPH as Gasoline EPA 5030 CA/L.UF1' 1 1 3/4/99 3/7/99 ND <br /> Benzene EPA 5030 8020 0 005 1 3/4/99 3/7/99 0 006 <br /> Toluene EPA 5030 8020 0 005 1 3/4/99 317/99 ND <br /> Ethylbenzene EPA 5030 8020 0 005 1 3/4/99 3/7/99 ND <br /> Xylenes Total EPA 5030 8020 0 005 1 3/4/99 3/7/99 ND <br /> Methyl tent-Butyl Ether EPA 5030 8020 005 1 3/4/99 3/7/99 ND <br /> is221020597p <br /> Page 30 <br />