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COLUMBIA ANALY'T'ICAL SERVICES,INC <br /> Analytical Report <br /> Client EMCON Service Request 59900683 <br /> Protect Apache Plastics/22640-100 001 Date Collected 2/24/99 <br /> Sample Matrix Soil Date Received 3/2/99 <br /> I <br /> I <br /> i <br /> BTEX,MTBE and TPH as Gasoline <br /> Sample Name 13-1(105) Units mg/Kg(ppm) <br /> Lab Code 59900683-009 Basis Wet <br /> "fest Notes <br /> Prep Analysis Dilution Date Date Result <br /> Analyte Method Method MRL Factor Extracted Analyzed Result Notes <br /> TPH as Gasoline EPA 5030 CAILUFT 1 5 3/4/99 3/7/99 13 <br /> Benzene EPA 5030 8020 0 005 5 3/4/99 3/7/99 079 <br /> Toluene EPA 5030 8020 0 005 5 3/4/99 3/7/99 3 7 <br /> Ethylbenzene EPA 5030 8020 0 005 5 3/4/99 3/7/99 0 36 <br /> Xylenes,Total EPA X030 8620 0 005 5 3/4/99 317/99 2 3 <br /> Methyl tert-Butyl Ether EPA 5030 8020 005 5 3/4/99 3/7/99 <0 25 C1 <br /> Cl Fbe MRL was elevated due to high analyte concentration requiring sample dilution <br /> 1S22/020597p <br /> 1 <br /> Page 29 <br />