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• <br />Al. Lancaster Laboratories Page 3 of 8 <br />. WhqTlMl� a-E&E�_o1 Summary <br />Client Name: Chevron Products Company Group Number: 793973 <br />Reported: 02/15/02 at 01:18 PM <br />Sample Matrix Quality Control <br />MS MSD M9/MSD RPD BKO DQP DUP Dup <br />Analysis NameRPD <br />RSC <br />1sRSC Limits RPD <br />MAX Conc Conc RPD <br />Max <br />Batch number: 02022A51 <br />Sample number(s): 3761185-3761203,3761207 <br />TPH-GRO - Waters <br />105 <br />74-132 <br />Benzene <br />116 <br />77-131 <br />Toluene <br />115 <br />80-128 <br />Ethylbenzene <br />115 <br />71-138 <br />Total Xylenes <br />115 <br />69-140 <br />Batch number: 020230024A <br />Sample number(s). 3761177-3761180 <br />Methanol (by Direct Injection) <br />104 <br />104 78-114 0 <br />20 <br />Batch number: 020230025A <br />Sample number(s): 3761181-3761184,3761166-3761200 <br />Methanol. (by Direct Injection) <br />100 <br />100 78-114 0 <br />20 <br />Batch number: 020280023A <br />Sample number(s): 3761201-3761206 <br />Methanol (by Direct Injection) <br />100 <br />100 78-114 0 <br />20 <br />Batch number: 020290025A <br />Sample <br />number(s): 3761185 <br />Methanol (by Direct Injection) <br />108 <br />106 78-114 0 <br />20 <br />Batch number: V020211AB <br />Sample. <br />number(s): 3761177-3761178 <br />hanol <br />88 <br />102 70-130 15 <br />30 <br />&thylt -butyl ether <br />102 <br />102 69-134 0 <br />30 <br />-Isopropyl ether <br />105 <br />105 68-133 0 <br />30 <br />Ethyl t -butyl ether <br />108 <br />107 73-123 1 <br />30 <br />t -Amyl methyl ether <br />104 <br />105 69-118 1 <br />30 <br />t -Butyl alcohol <br />100 <br />101 51-148 1 <br />30 <br />1,2-Dichloroethane <br />108 <br />108 75-141 0 <br />30 <br />1,2-Dibromoethane <br />99 <br />102 78-120 3 <br />30 <br />Batch number: V020212AA <br />Sample <br />number(s): 3761179-3761188 <br />Ethanol <br />103 <br />101 70-130 2 <br />30 <br />Methyl t -butyl ether <br />100 <br />101 69-134 0 <br />30 <br />di -Isopropyl ether <br />100 <br />98 68-133 2 <br />30 <br />Ethyl t -butyl ether <br />108 <br />107 73-123 2 <br />30 <br />t -Amyl methyl ether <br />101 <br />100 69-118 1 <br />30 <br />t -Butyl alcohol <br />104 <br />103 51-148 1 <br />30 <br />1,2-Dichloroethane <br />109 <br />109 75-141 0 <br />30 <br />1,2-Dibromoethane <br />100 <br />101 78-120 1 <br />30 <br />Batch number: V020212AB <br />Sample <br />number(s): 3761189-3761196 <br />Ethanol <br />103 <br />101 70-130 2 <br />30 <br />Methyl t -butyl ether <br />100 <br />101 69-134 0 <br />30 <br />di -Isopropyl ether <br />100 <br />98 68-133 2 <br />30 <br />Ethyl t -butyl ether <br />108 <br />107 73-123 2 <br />30 <br />t -Amyl methyl ether <br />101 <br />100 69-118 1 <br />30 <br />t -Butyl alcohol <br />104 <br />103 51-148 1 <br />30 <br />1,2-Dichloroethane <br />109 <br />109 75-141 0 <br />30 <br />1,2-Dibromoethane <br />100 <br />101 78-120 1 <br />30 <br />Batch number: V020221AA Sample number(s): 3761197-3761206 <br />*- Outside of specification <br />1) The result for one or both determinations was less than five times -the LOQ. <br />The background result was more than four times the spike added. <br />Lancaster Laboratories, Inc. <br />MEMBER 2425 New Holland Pike <br />PO Box 7 <br />La <br />� Lancasterr,, PA PA 17605-2425 <br />717.656-2300 Fax: 717-656-2681 <br />2216 Rev. 9/11/00 <br />