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• <br />J Lancaster Laboratories Page 4 of 8 <br />Whe&l�dvyaConrol Summary <br />Client Name: Chevron Products Company Group Number: 793973 <br />Reported• —1 <br />GalYsiS Name: TPH-GRO - 'Waters <br />Batch number: 02021A02 <br />Trifluorotoluene-F <br />3761204 99 <br />3761205 99 <br />3761206 100 <br />Blank 98 <br />LCS 114 <br />LCSD 110 <br />Ms 111 <br />Limits: 67-135 <br />Analysis Name: TPH-GRO - Waters <br />Batch number: 02022ASS <br />Trifluorotoluene-F <br />3761177 96 <br />3761178 97 <br />3761179 95 <br />3761180 94 <br />3761181 95 <br />3761182 97 <br />3761183 96 <br />3761184 96 <br />Blank 98 <br />LCS 108 <br />Surrogate Quality Control <br />Trifluorotoluene-P <br />1D3 <br />97 <br />100 <br />101 <br />100 <br />100 <br />102 <br />71-130 <br />Trifluorotoluene-P <br />86 <br />87 <br />86 <br />85 <br />86 <br />87 <br />87 <br />87 <br />86 <br />85 <br />*- Outside of specification <br />1 The result for one or both determinations was less than five times the LOQ. <br />The background result was more than four times the spike added. <br />Lancaster Laboratories, Inc. <br />MEMBER 2425 New Holland Pike <br />La Box 12425 <br />La <br />� ncaster, PA <br />17605-2425 <br />717-656-2300 Fax. 717-656-2681 <br />DUP Dup <br />RPD <br />RPD Max <br />2216 Rev. 9/11/00 <br />at 01:18 Phi <br />Sample Matrix <br />Quality Control <br />MS <br />MSD <br />M9/MBD <br />RPD BACs DUP <br />Analysis Name <br />Ethanol <br />$RSC <br />%REC <br />Limits <br />RPD MAIC Conc Conc <br />Methyl t-butyl.ether <br />102 <br />101 <br />99 <br />99 <br />70-130 <br />3 <br />30 <br />di-ieopropyl.ether <br />101 <br />100 <br />69-134 <br />68-133 <br />2 <br />30 <br />Ethyl t -butyl. ether <br />101 <br />103 <br />73-123 <br />0 <br />3 <br />30 <br />30 <br />t -Amyl methyl ether <br />98 <br />100 <br />69-118 <br />2 <br />30 <br />t-Butyl.alcohol <br />103 <br />98 <br />51-148 <br />5 <br />30 <br />1,2-Dichloroethane <br />110 <br />108 <br />75-141 <br />1 <br />30 <br />1,2-Dibromoethane <br />100 <br />98 <br />78-120 <br />1 <br />30 <br />Batch number; V020221AB <br />Ethanol <br />Sample <br />number(s).- <br />3761205 <br />di -Isopropyl ether <br />102 <br />101 <br />99 <br />100 <br />70-130 <br />3 <br />30 <br />Ethyl t -butyl ether <br />101 <br />103 <br />68-133 <br />73-123 <br />0 <br />3 <br />30 <br />t -Amyl methyl ether <br />98 <br />100 <br />69-118 <br />2 <br />30 <br />30 <br />t -Butyl. alcohol <br />103 <br />98 <br />51-148 <br />5 <br />30 <br />1,2-Dichloroethane <br />110 <br />108 <br />75-141 <br />1 <br />30 <br />1,2-Dibromoethane <br />100 <br />98 <br />78-120 <br />1 <br />30 <br />GalYsiS Name: TPH-GRO - 'Waters <br />Batch number: 02021A02 <br />Trifluorotoluene-F <br />3761204 99 <br />3761205 99 <br />3761206 100 <br />Blank 98 <br />LCS 114 <br />LCSD 110 <br />Ms 111 <br />Limits: 67-135 <br />Analysis Name: TPH-GRO - Waters <br />Batch number: 02022ASS <br />Trifluorotoluene-F <br />3761177 96 <br />3761178 97 <br />3761179 95 <br />3761180 94 <br />3761181 95 <br />3761182 97 <br />3761183 96 <br />3761184 96 <br />Blank 98 <br />LCS 108 <br />Surrogate Quality Control <br />Trifluorotoluene-P <br />1D3 <br />97 <br />100 <br />101 <br />100 <br />100 <br />102 <br />71-130 <br />Trifluorotoluene-P <br />86 <br />87 <br />86 <br />85 <br />86 <br />87 <br />87 <br />87 <br />86 <br />85 <br />*- Outside of specification <br />1 The result for one or both determinations was less than five times the LOQ. <br />The background result was more than four times the spike added. <br />Lancaster Laboratories, Inc. <br />MEMBER 2425 New Holland Pike <br />La Box 12425 <br />La <br />� ncaster, PA <br />17605-2425 <br />717-656-2300 Fax. 717-656-2681 <br />DUP Dup <br />RPD <br />RPD Max <br />2216 Rev. 9/11/00 <br />