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GeoAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209) 572-0900 Fax (209) 572-0916 <br /> Report# Q338-05 CERTIFICATE OF ANALYSIS Date: 12/09/04 <br /> Date Rec'd: 12/03/04 <br /> Thorpe Oil Date Started: 12/07/04 <br /> PO Box 357 Project: 216 N. California Street Date Completed:12/08/04 <br /> Lodi CA 95241 Date Sampled: 12/03/04 <br /> PO# Time: 1:31 pm <br /> Sample ID: South Sampler ; O.Sanchez(Geo) <br /> Lab ID: Q201812 <br /> Method RL Analyte Results Units <br /> 8260B 500 Benzene ND µg/Kg <br /> 500 Toluene ND <br /> 500 Ethyl Benzene ND <br /> 500 Total Xylenes ND <br /> 1000 - Methyl tert-butyl ether(MTBE) ND <br /> i <br /> 40000 Ethanol ND <br /> 20000 tert-Butanol ND - -, <br /> 1000 di-Isopropyl ether(DIPE) ND <br /> 1000 Ethyl tert-butyl ether(ETBE) NO - <br /> 1000 tert-Amyl methyl ether(TAME) ND <br /> i <br /> i <br /> Surrogate Amnt Spiked Amnt Rec %Recovery QC Limit% <br /> *Elevated Reporting limits due to high level of 1,2-Dichloroethane-d, 2000 1960 98.0 66-133 <br /> non-target analytes 2-Bromo-l-chloropropane 2000 2090 104.5 63-139 <br /> 4-Bromofluorobenzene 2000 1970 98.5 64-136 <br /> � I?�-[ <br /> Mario D'Onofri� Donna Keller <br /> hams ct Certification # 2585 Tarn oyy, Dir@ftor <br />