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GeoAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone(209)572-0900 Fax(209) 572-0916 <br /> Report# Q338-05 CERTIFICATE OF ANALYSIS Date: 12/09/04 <br /> Date Rec'd: 12/03/04 <br /> Thorpe Oil Date Started: 12/07/04 <br /> PO Box 357 project: 216 N. California Street Date Completed:l2/08/04 <br /> Lodi CA 95241 Date Sampled: 12/03/04 <br /> Pp# Time: 129pm <br /> Sample ID: North Sampler: O.Sanchez(Geo) <br /> Lab ID: Q201811 <br /> Method RL Analyte Results Units <br /> 8260B 500 Benzene ND µg/Kg <br /> 500 Toluene ND <br /> 500 Ethyl Benzene ND <br /> 500 Total Xylenes ND <br /> 1000 Methyl ten-butyl ether(MTBE) ND <br /> 40000 Ethanol ND <br /> 20000 tert-Butanol ND <br /> 1000 di-Isopropyl ether(RIPE) ND - <br /> 1000 Ethyl tert-butyl ether(ETBE) ND <br /> 1000 tert-Amyl methyl ether(TAME) ND <br /> }t <br /> i <br /> Surrogate Amnt Spiked Amnt Rea %Recovery OC Limit% <br /> -Elevated Reporting limits due to high level of 1,2-Dichloroethane-d4 2000 1964 98.2 66-133 <br /> non-target analytes 2-Bromo-l-chloropropane 2000 1889 94.5 63-139 <br /> 4-Bromofluorobenzene 2000 2300 115.0 64-136 <br /> a, LCL'-� <br /> Mario D,OnofTib Donna Keller <br /> Chemist Certification # 2585 Laboratory Director <br />