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GeoAnalytical Laboratories, Inc <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone(209)572-0900 Fm(209)572-0916 <br /> Report# S6C2008 Project: 835 N. Central Date: 03/30/06 <br /> Thorpe Oil Date Rec'd: 03/20/06 <br /> PO Box 357 PO# <br /> Lodi,CA 95241 <br /> CERTIFICATE OF ANALYSIS <br /> Sample ID: Pit Water Date Sampled: 03/20/06 <br /> Lab ID: S6C2008-04 Time: 13:37 <br /> Volatile Organic Chemistry of Hazardous Waste Sampler: Oscar Sanchez <br /> Method RL Analyte Result Units Notes Analyzed Batch# <br /> 82608 120 Benzene 625 ug/L 03/22/06 S001101 <br /> 120 Toluene 9930 ug/L <br /> 120 Ethylbenzene 1950 ug/L <br /> 240 Xylenes,total 3580 ug/L <br /> 5030/LUFT 10.0 Gasoline 39.3 mg/L 03/22/06 S001098 <br /> Surrogate Amnt Spiked Amnt Recovered %Recovery QC Limit% Surrogate Notes <br /> a,a,a-Trifluorotoluene 5000 4330 87% 70-125 <br /> 1,2-Dichloroethanc-d4 2000 2040 102% 72-132 <br /> 2-Bromo-I-Chloropropme 2000 1880 94% 71-134 <br /> 4-Bmmolluorobenzene 2000 2020 101 % 74-132 <br /> vF41 -1�K#4 <br /> Mario 'Onofrio Donna Keller <br /> Chemist Laboratory Director <br /> Certification#2585 <br />