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Geo�vnalytical Laboratories;-inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209) 572-0900 Fax(209) 572-0916 <br /> Report# P085-16 CERTIFICATE OF ANALYSIS Date: 4/02/03 <br /> Thorpe Oil Date Rec'd: 3/26/03 <br /> Date Started: 4/01/03 <br /> PO Box 357 Project: Tank Pull @ 2944 S. Airport-Stockton Date Completed:4/01/03 <br /> Lodi CA 95241 <br /> Date Sampled: 3/26/03 <br /> PO# Time: 2:19pm <br /> Sample ID: TK-2 @10' Sampler : R.Azevedo(Geo) <br /> Lab ID: P200483 <br /> Method RL Analyte Results Units <br /> 8260B 10 Methyl tert-butyl ether(MTBE) ND <br /> µg/Kg <br /> 400 Ethanol ND <br /> 200 tert-Butanol ND <br /> 10 di-Isopropyl ether(DE'E) ND <br /> 10 Ethyl tert-butyl ether(ETBE) ND <br /> 10 tert-Amyl methyl ether(TAME) ND <br /> 10 Ethylene dibromide(EDB) ND <br /> 5.0 1,2-Dichloroethane(1,2-DCA) ND <br /> Surrogate Amnt Spiked Amnt Rec. %Recovery QC Limit% <br /> 1,2-Dichloroethane-d4 20 25.3 126.5 66-133 <br /> 2-Bromo-l-chloropropane 20 20.3 101.5 63-139 <br /> 4-Bromofluombenzene 20 20.7 103.5 64-136 <br /> ��i� <br /> Mario D'Ond io Donna Keller <br /> Chemist Certification # 1157 Laboratory Director <br />