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Geomialytical Laboratories,-incc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209) 572-0900 Fax (209) 572-0916 <br /> Report# P085-16 CERTIFICATE OF ANALYSIS Date: 4/02/03 <br /> Thorpe Oil Date Recd: 3/26/03 <br /> Date Started: 4/01/03 <br /> POBox357 Project: Tank Pull @29445. Airport-Stockton Date Completed:4/01/03 <br /> Lodi CA 95241 <br /> Date Sampled: 3/26/03 <br /> PO# Time: 2:37pm <br /> Sample ID: SP- 1 (Stock Pile) Sampler : R.Azevedo(Geo) <br /> Lab ID: P200484 <br /> Method RL Analyte Results Units <br /> 8260B 10 Methyl tert-butyl ether(MTBE) ND µg/Kg <br /> 400 Ethanol ND <br /> 200 tert-Butanol ND <br /> 10 di-Isopropyl ether(RIPE) ND <br /> 10 Ethyl tert-butyl ether(ETBE) ND <br /> 10 tert-Amyl methyl ether(TAME) ND <br /> 10 Ethylene dibromide(EDB) ND <br /> 5.0 1,2-Dichloroethane(1,2-DCA) ND <br /> Surrogate Amnt Spiked Amnt Rec. %Recovery OC Limit% <br /> 1,2-Dichloroethane-d4 20 26.3 131.5 66-133 <br /> 2-Bromo-l-chloropropane 20 21.1 105.5 63-139 <br /> 4-Bromofluorobenzene 20 20.4 102.0 64-136 <br /> v'4-,(("� <br /> azto D Donna Keller <br /> Chemist Certification #1157 Laboratory Director <br />