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W702 ENVIRONMENTAL HEALTH TITLE 22 <br /> (p• 1800.82) I11691stor U.No.7^1.12!6) <br /> water equivalent to that of the Initial Filtrate. These procedures shall be fol- <br /> lowed prior to acidification of Treatment and Blank solutions with nitric acid <br /> to five percent (by volume) acid content. The bottle shall then be stored at <br /> room temperature or frozen. If the extracts are also to be analyzed for the <br /> organic substances listed in Section 66699(c),or for the organic substances only, <br /> the filtered extracts shall be transferred to clean glass bottles.If the extracts are <br /> to be analyzed for fluoride, they shall be transferred to clean polyethylene <br /> bottles.These extracts,containing organic substances or fluoride,shall not be <br /> acidified,but shall be frozen soon after each extract is obtained and held frozen <br /> until the day of analysis, unless the extracts are analyzed within 24 hours. <br /> (g) Sample analysis and data treatment shall be as follows: <br /> (1) Each of the filtered extracts from the Treatment and Blank extractions <br /> shall have been acidified to five percent by volume nitric acid, and stored at <br /> room temperature or frozen in polyethylene bottles or kept frozen without <br /> addition of acid in glass bottles until the day of analysis,as prescribed.Each of <br /> the extracts shall be thoroughly mixed just prior to being individually analyzed <br /> for the substances listed in Section 66699 in order to determine whether the <br /> extractable concentration (EC) in the waste or other material exceeds the <br /> MC for any of the substances listed.The extracts shall be analyzed according <br /> to the procedures identified in Sections 66700(6)(2), (b) 3) and (b)(4). <br /> (2) The net EC of a substance in the Treatment sample which is listed in <br /> Section 66699 shall be calculated and reported as milligrams per liter of sample <br /> (mg/1). This value is derived after subtracting the concentration of the sub- <br /> stance in the appropriate Blank extract from that concentration determined in <br /> the Treatment extract. <br /> NOTE: Authority cited: Sections 208,25141 and 25150, Health and Safety Code. Refer- <br /> ence:Section 25141,Health and Safety Code. <br /> HISTORY: <br /> 1. Editorial correction filed 10-5-84;designated effective 10-27$4 (Register 84,No.41). <br /> 66702. Ignitabitity Criteria. <br /> (a) A waste, or a material, is ignitable and hazardous if it: <br /> (1) Is a liquid,other than an aqueous solution containing less than 24 percent <br /> alcohol by volume, and has a flash point less than 60 degrees centigrade (140 <br /> degrees Fahrenheit),as determined by a Pensky-Martens Closed Cup Tester, <br /> using the test method specified in American Society for Testing and Materials <br /> (ASTM) Standard D-93-79, or a Setaflash Closed Cup Tester, using the test <br /> method specified in ASTM Standard D-3278-73; or <br /> (2) Is not a liquid and is capable,under standard temperature and pressure, <br /> of causing fire through friction,absorption of moisture or spontaneous chemical <br /> _ changes and,when ignited,burns so vigorously and persistently that it creates <br /> a hazard; or <br /> (3) Is a flammable compressed gas as defined in 49 CFR 173.300(6) (codified <br /> October 1, 1982) and as determined by the test methods described in that <br /> regulation; or <br /> (4) Is an oxidizer as defined in 49 CFR 173.151 (codified October 1, 1982). <br /> NOTE:Authority cited: Sections 208,25141 and 25150, Health and Safety Code. Refer. <br /> _ ence: Section 25141, Health and Safety Code. <br />