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i <br /> yII)Vt VERIFICATION LABORATORY ANALYSIS <br /> O:tYGEYAiES `IE,t,ALS PCB <br /> (MTBE. <br /> TP - TE CL HC TOTAL MTBE TBA DI <br /> HG TPH-D BX & PS ICAP/ 8270 <br /> TANK TANK 8015 8 8010 LEAD 8020 ETRE, AES g <br /> # p80 <br /> CONTENTS 8015 <br /> 8260 8260 8260 8240 742082 8260 °AA <br /> 8260 74211 <br /> X X X <br /> LEADED GAS X X <br /> X <br /> UNL GAS X - <br /> X <br /> DIESEL X y <br /> X <br /> KEROSENE X X X <br /> X <br /> !� UNK FUEL X X X <br /> PROD. OIL <br /> X X <br /> X <br /> CHLOR. X X <br /> SOLVENTS <br /> X <br /> NONCHLOR X X <br /> SOLVENTS <br /> X X <br /> WASTE\ X X X X <br /> USED OIL X <br /> Appendix D (B),Table 3-5 on page A20 for <br /> All analysis methods aze the designated EPA methods described in EPA SW 846,Third Edition. Those methods not found in S <br /> 846 are specifically noted below. Refer to the "SWRCB LUFT Field Manual", APP <br /> min mum detection limits for motor vehicle fuel(gasoline and diesel). Refer to "Tri-Regional Board Staff Recommendations for <br /> Initial Evaluation and Investigation of UST's" for the waste and motor oil minimum detection limits. <br /> however Limits th shall utilize the mosMCL, <br /> conservative r All odable Limit of the contaminant in accepted, <br /> question will be <br /> tection LABORATORY ANALYSES TERMINOLOGY: <br /> TPH-G Total Petroleum Hydrocarbon, Gasoline,GC/FID(5030)8015 mod or GC/MS 82 <br /> 60 <br /> TPH-D Total Petroleum Hydrocarbon,Diesel, GC/FID(3550), 8015 mod or GC/MS 8260 <br /> BTX&E Benzene,Toluene,Xylene&Ethyl Benzene,GC/PID 8020 or GC/MS 8260 <br /> Chlorinated Hydrocarbon, GC/HSD 8010, GC/MS 8240 or 8260 <br /> CL HC 7420 AA 7421 or ICP-AES 6010 <br /> TOTAL LEAD Total lead, AA <br /> OXYGENATES MTBE,ETBE,TAME, DB?E, &TBA GC/MS 8260(For MTBE screen only you may use 8 <br /> 020) <br /> METALS ICAP or AA Inductively Coupled Plasma Atomic Emissio Spectra Zinc and N'�OCkeL[omit Absorption Spectrometry 7000. <br /> Metals: Cadmium,Chromium III and VI, <br /> PCB Polychlorinated Biphenyls,GC/MS 8270 or 8080 <br /> GC-FID <br /> Gas Chromatography, Flame Ionization Detection <br /> Method 3050 Acid digestion <br /> Method 3540 <br /> Soxhlet sample preparation <br /> Method 3550 Sonication sample preparation, extraction meth <br /> od <br /> Method 5030 Purge and trap sample preparation <br /> QA/QC Quality Assurance/Quality Control <br /> free <br /> cked <br /> Notes: Toa id false <br /> acolumn maydetection <br /> be asf a benzene, <br /> ,benzithene- <br /> t wl "dirty"sam lesvents rortonc the hydrocarbons havcolumns en characterized preferred <br /> dnd pto roper <br /> Y" P <br /> columns: packed the <br /> QA/QC is followed. require further analysis. <br /> For drinking water sources, EPA re <br /> detection <br /> the <br /> 5pes exhibiting any levelof heavy metal c nttaminadon may req ice to the 600 fererpries because <br /> detection limits are lower and the those <br /> sQAJQles until disposal is indicated. <br /> PHS-£HD recommends holding those samples <br /> Page 8 <br /> EH 23 046 (Revised 05/09/00) <br />