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MINIMUM VERIFICATION LABORATORY A? kLYSLS <br /> TANK 11 TANK TPH-G TPH-D BTX &E CL HC TOTAL EDB METALS PCB <br /> C0N'I'Ea`1TS 3015 8015 3020 8010 LEAD ICRP/ 3270 <br /> 8260 8260 8260 3240 7420 8240 AES or 8030 <br /> 7421 AA <br /> LEADED <br /> GAS X X X X <br /> UNL GAS X X <br /> DIESEL X J X <br /> =ROSENE X X <br /> LTLNFK FUEL X X X X I X <br /> PROD. OIL I X I X <br /> OLVEN—IS I X X <br /> E. <br /> NONSOL C.N�R I I X I X X <br /> W.a,ST— <br /> USED O? I X I X X C I I I X X <br /> ,Ail analyses m.thcds are designated EPA methods descncoed in EPA SW 3'6,Taird Edition. Those methods not found <br /> in SW 3=6, are ape_Ecaliv noted below. Refer to the 'SWRCB LLQ Fled Manual', Appendix A-20, Table 3-5 for <br /> dere^ion limits of motor vehicle fuels (gasoline and diose;). Refer ro 1-2-3 'R.gional Board Staff Racommendaaors far <br /> rniaal Evaluation and Investigation of U5 T s' for the waste and motor od deteeioa limits. <br /> Detection Limits that remain below the MCL, STLC or:Ulowable Limit of the contaminant in question will be accepted, <br /> ho,•ever laboratory shatl utilize the most conservative method. <br /> La30EZ_�7CRY A N.-k.LYSES i=RN[LNOLOGY: <br /> T?H-G Total Petroleum Hydroctrboa, Gasoline, CC,= (5030) 3015 mod or GCMS 3260 <br /> TPH-D Total Petroleum Hydrocarboa, Diesel, GG'Fm (3550), 3015 mod or GCjNMS 3250 <br /> BTX & E Benzene, Toluene, Xylene & Ethyl Benzene, GCIPM 3020 or GCIMS 8260 <br /> CL HC Chlorinated Hydrocarbon, GC'HSD 8010, GGMS 3240 <br /> TOTAL, LEAD Total lead, AA 7420, AA 7421 or IC?-AES 6010 <br /> EDB Ethylene dibromide (DHS-AB 1803), GCIMS 3240 (DHS-LUFT) <br /> CC-FID Gas Chromatography, Flame Ionization Detectica <br /> ICA? or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorpdoa <br /> Spectrometry 7000. Metals: Cadmium, Chromium III and VT, Lead, Zinc and Nickel. <br /> PCB Polychlorinated Biphenyls, GGMS 3270 or 3030 <br /> Methad 3050 Acid digestion <br /> Method 3540 Soxhlet sample preparation <br /> Method 3550 Sonication sample preparation, extracdca method <br /> Nfethod 5030 Purge and trap sample preparation <br /> QA/QC Quality Assnranc::'Quaiitp Control <br /> Notes: To avoid false positive detection of benzene, benzene-free solvents are to be used. Fussed apUlary columns are <br /> preferred to packed columns; a packed column may be used as a 'first c C with 'dirty"samples or once the hydrocarbons <br /> have been characterized and proper QA/AC is followed <br /> For Drinking water sources, EPA remmmeads that the 500 series for volatile organics be used in preference to the 600 <br /> series because the detection limits are Iower and the QA/QC is better. Samples exhibiting any level of heavy metal <br /> contamination may require further analysis. PHS-EI-M recommends holding these samples until disposal is indicated. <br /> E:-( '-)3 043 (Revised 7/I0i92) Page 3 <br />