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SAN .70A*IPJ LOCAL, <br />MININLM VERIFICATION LABORATORY ANALYSIS <br />TANK CON7ENI'S - TPH-G TPH-D <br />Waste Product OC -FID GC -FID <br />or- —.- (5030) (5030) <br />TEPH <br />(3550) <br />(3540) <br />BTUE <br />(8020) <br />CL HC <br />(8010) <br />(8240) <br />TEL <br />(D <br />Total Extractable Petroleum Hydrocarbon (8015) <br />(8020) <br />CI. HC 8010 OR 8240 <br />Benzene, Toluene, Xylene b Ethyl Benzene (8020) <br />EDB <br />H S) <br />METALS <br />(ICP- <br />AEg) <br />PCB <br />(8270) <br />LEADED GASOLINE x <br />- <br />X <br />OC FID <br />ICP -AES DR AA <br />x <br />x <br />Inductively Coupled Plasma Atomic E}nission Spectrometry or Atomic <br />UNL GASOLINE x <br />Method 5030 <br />x <br />Method 3550 <br />Sonication Sample Preparation <br />Method 3540 <br />Soxhlet Sample Preparation <br />QA/0C <br />DIL'M <br />x <br />x <br />KHMENE x <br />x <br />L"CNM FUEL x <br />x <br />x <br />x <br />x <br />OIL <br />x <br />x <br />CHLOR. SOLVENTS <br />x <br />x <br />NONCHL R. SOLVTS <br />x <br />- <br />WASTE/USED OIL <br />x <br />x <br />x <br />x <br />x <br />MINIMUM VERIFICATION LABORATORY ANALYSES T RMINOLOGy <br />The following listing of laboratory analyses abbreviations is provided as a guide so that <br />terminology used will be more familiar. All analyses methods are designated EPA methods as <br />described in EPA SN 846, Third Edition. Those methods not found in SW 846, are <br />specifically noted. <br />TPH G <br />TPH D <br />Total Petroleum Hydrocarbon, Gasoline <br />Total Petroleum Hydrocarbon, Diesel <br />TNPH <br />BTX i E <br />Total Extractable Petroleum Hydrocarbon (8015) <br />(8020) <br />CI. HC 8010 OR 8240 <br />Benzene, Toluene, Xylene b Ethyl Benzene (8020) <br />TEL (DOHS-LUFT) <br />Chlorinated Hydrocarbon 8010 or 8240 <br />Tetraethyl Lead (DOHS-LUFT) <br />EDB (DONS -AB 1803) <br />Ethylene dibromide (DOHS -AB 1803) <br />OC FID <br />ICP -AES DR AA <br />Gas Chromatography, Flame Ionization Detector <br />Inductively Coupled Plasma Atomic E}nission Spectrometry or Atomic <br />Absorption Spectrometry <br />Method 5030 <br />Purge and Trap Sample Preparation <br />Method 3550 <br />Sonication Sample Preparation <br />Method 3540 <br />Soxhlet Sample Preparation <br />QA/0C <br />Quality Assurance/Quality Control <br />Notes: To avoid false positive detection of benzene, benzene -free solvents are to be used. <br />?used capillary columns are preferred to packed columns; a packed column nay be used as a <br />"first cut" vJth "dirty" samples or once the hydrocarbons have been characterized and <br />Proper QA/QC is followed. <br />For Drinking Nater Sources, EPA recommends that the 500 series for volatile <br />organics be used In preference to the 600 series because the detection limits are lover and <br />the QA/QC is better. <br />SITE ADDRESS_ 25499 E. Shelton Rd., Linden, CA Sweeps H <br />Eii 23 048 12/88 Contractor: JIM THORPE OIL,_ INC. Approval date <br />