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L L January 22, 2004 Lab ID STK338235 Toto Newhall Customer : 3-15180 Quality Control - Inorganic L Constituent Method Date/ID Type Units br i QC Data DQO Note Metals Cadmium 6010B O1/07/2004:A 02-CCB mg/L ND <0.005 L 02-CCV mg/L 1.000 101% 90-110 03-CCB mg/L ND <0.005 03-CCV mg/L 1.000 106% 90-110 L Chromium 3050B O1/07/2004:A209 Blank mg/kg ND <0.5 LCS mg/kg 40.00 101% 85-115 PDS mg/kg 40.00 103% 75-125 MS mg/kg 40.00 92.8% 75-125 L (SP 313835-01) MSD mg/kg 40.00 97.2% 75-125 MSRPD mg/kg 4.1% 520 6010B 01/07/2004:A 02-CCB mg/L ND <0.01 L 02-CCV mg/L 1.000 9LS% 90-110 03-CCB mg/L ND <0.01 03-CCV mg/L 1.000 104% 90-110 Cuiwlt 3050B 01/07/2004:A209 Blank mg/kg ND <0.5 I LCS mg/kg 40.00 103% 85-115 L, PDS mg/kg 40.00 108% 75-125 MS mg/kg 40.00 96.6%. 75-125 (SP 313835-01) MSD mg/kg 40.00 99.1%, 75-125 MSRPD mg/kg 2.5% 520 6. 601(1B 01/072004:A 02-CCB mg/L ND <0-0 (12-CCV mg/L 1.(1(10 99.7% 9(1-]](1 03-CCB mg/L ND <0.01 03-CCV mg/L 1.000 1099, 90-1111 Copper 3050B 011072004:A209 Blank mg/kg ND <0.5 LCS mg/kg 40.00 99.3%. 85-115 PDS mg/kg 40.00 103% 75-125 6. MS mg/kg 40.00 112% 75-125 . �. (SP 313835-01) MSD mg/kg 40.00 159% 75-125 435 MSRPD mg/kg 14.8% 520 STLC 01/12/2004:8217 ExBlk mg/L 0.0030 0.0100 h. PDS mg/L 0.8200 616% <'A ExDup mg/L 02% 20 01/21/2004:A217 ExBlk mg/L 0.016 0.0100 210 ` PDS mg/L 1.025 79.3% 75-125 ExDup mg/L 9.4% 20 6010B O1/07/2004:A 02-CCB mg/L ND <0.01 ` 02-CCV mg/L 1.000 99.1% 90-110 03-CCB mg/L ND <0.01 03-CCV mg/L 1.000 103% 90-110 O1/0912004:C 00-1CB mg/L ND <0.01 220 01-CCB mg/L ND <0.01 O1/21/2004:A 00-ICB mg/L ND <0.01 00-ICV mg/L 1.000 101% 90-110 L Report continued on next page... STK338235: Quality Control Page 2