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January 22, 2004 Lab ID : STK338235 Tom Newhall Customer : 3-15180 L Quality Control - Inorganic `. Constituent Method Date/ID Type Units Cone. QC Data DQO Note L FMIletals6UlOB Ul/21/2004:.0 Ol-CCB mg/L ND <0.01 O1-CCV mg/L 1.000 1015% 90-110 3050B O1/07/2004:A209 Blank mg/kg ND <0.5 LCS mg/kg 40.00 101% 85-115 L PDS mg/kg 40.00 103% 75-125 MS mg/kg 40.00 95.4% 75-125 (SP 313835-01) MSD mg/kg 40.00 96.7% 75-125 MSRPD mg/kg 1.3% 1520 L 6010B O110712004:A 02-CCB mg/L ND <0.01 02-CCV mg/L 1.000 99.2% 90-110 03-CCB mg/L ND <0.01 03-CCV mg/L 1.000 106% 90-110 LMercury 7471A 01/08/2004:A212 Blank mg/kg ND <0.03 LCS mg/kg 02775 106% 85-115 L MS mg/kg 0.2778 124% 75-125 (SP 313776-0I) MSD mg/kg 02778 105% 75-125 MSRPD mg/kg 11.5%. 520 7471A 01/08/21N14:A 00-112B ug/L ND <ll.] L0()-ICV ug/L 4.167 99A%. 90-110 01-CCB ug/L ND <O.1 (11-CCV ug/L 4.167 100% 90-110 L Molybdenum 30500 01/07/2004:A209 Blank nig/kg ND <0.5 LCS mg/kg 25.00 99.0% 85-115 PDS mg/kg 25.00 1029 75-125 MS nig/kg 25.00 90,7%, 75-125 (SP 313835-01) MSD mg/kg 25.00 98.5% 75-125 MSRPD nig/kg 7.3% <20 L 6010B 01/07/2004:A 02-CCB mg/L ND <0.01 02-CCV mg/L 1.000 98.0% 90-110 03-CCB mg/L ND <0.01 L03-CCV mg/L 1.000 105% 90-110 Nickel 3050B O110712004:A209 Blank mg/kg ND <0.5 LCS mg/kg 40.00 102% 85-115 { PDS mg/kg 40.00 104% 75-125 L MS mg/kg 40.00 93.3% 75-125 (SP 313835-01) MSD mg/kg 40.00 100% 75-125 MSRPD mg/kg 6.3% <_20 6010B O1107/2004:A 02-CCB mg/L ND <0.01 L 02-CCV mg/L 1.000 101% 90-110 03-CCB mg/L ND <Ml 03-CCV mg/L 1.000 106% 90-110 LSelenium 30508 0110712004:.0209 Blank mg/kg ND <0.5 LCS mg/kg 40.00 95.3% 85-115 PDS mg/kg 40.00 98.1% 75-125 LMS mg/kg 40.00 86.1% 75-125 Report continued on next page... L STK338235: Quality Control Page 3 L