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6. January 22, 2004 Lab ID : STK338235 Tom Newhall Customer : 3-15180 L Quality Control - Inorganic 6. I Constituent Method Date/ID Type Units Cone. QC Data DQO Note Metals Selenium 3050B Ol/07/2004:A209 MSD mg/kg 40.00 90.5% 75-125 ` MSRPD mg/kg 4.8% 520 6010B 01/15/2004:A 02-CCB mg/L ND <0.01 02-CCV me/L 1.000 98.5% 90-110 03-CCB - mg/L ND <0.01 03-CCV mg/L 1.000 101% 90-110 Silver 3050B 01/07/2004:A209 Blank mg/kg ND <0.5 LCS mg/kg 40.00 97.0% 85-115 PDS mg/kg 40.00 101% 75-125 MS mg/kg 40.00 78.95 75-125 (SP 313835-01) MSD mg/kg 40.00 92.0% 75-125 MSRPD mg/kg 139% 520 L 6010B 01/07/2004:A 02-CCB mg/L ND <0.01 02-CCV mg/L 1.000 98.1% 90-110 03-CCB mg/L ND <0.01 L03-CCV mg/L 1.000 98.8''% 90-110 Thallium 3050B (11/(17/2(104:A209 Blank rug/kg ND <0.5 LCS mg/kg 40.00 98.1%, 85-115 PDS mg/kg 40.O0 101% 75-125 L75-125 MS mg/kg 40.00 x8.2%. (Sl' 313835-01) MSD mg/kg 40.00 91.4% 75-125 MSRPD mg/kg 3.6%. <20 6010B 01/162004:A OUdCB mg/L ND <0.01 00-ICV m,,/l, 1.000 101% 95-105 O]-CCB mg/L ND <0.01 01-CCV mg/L 1.000 104%, 90-110 Vanadium 3050B O1/0712004:A209 Blank mg/kg - ND <0.5 LCS mg/kg 40.00 99.4% 85-115 PDS mg/kg 40.00 102% 75-125 MS mg/kg 40.00 92.5% 75-125 (SP 313835-01) MSD mg/kg 40.00 96.7% 75-125 MSRPD mg/kg 4.2% <20 6010B 01/07/2004:A 02-CCB mg1L ND <0.01 02-CCV mg/L 1.000 98.5% 90-110 L 03-CCB mg/L ND <0.01 03-CCV mg/L 1.000 102% 90-110 Zinc 3050B O1/0712004:A209 Blank mg/kg ND <1 L LCS mg/kg 40.00 106% 85-115 PDS mg/kg 40.00 101% 75-125 MS mg/kg 40.00 103% 75-125 (SP 313835-01) MSD mg/kg 40.00 158% 75-125 435 MSRPD mg/kg 15.4% <20 L 6010B 01/15/2004:A 02-CCB mg/L ND <0.02 02-CCV mg/L 1.000 98.5% 90-110 03-CCB I mg/L ND 1 <0.02 Report continued on next page... ►. STK338235: Quality Control Page 4 L