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TONENGINEERING *240811 <br /> P. 09 <br /> MRR is '93 03:20PM ULTRAMRR INC. <br /> P.9116 <br /> NMk; M`'ERIPICATION LABORATORY ANALYSIS <br /> TANK TANK TPH-G TPH-D BTX tit E CL HC TOTAL EDB <br /> CON' tNT5 8017 9015 8020 8010 METALS PCS . <br /> sw 8250 g EZ4o <br /> ICA?/ <br /> 8270 <br /> 7420 3240 AES or 8080 <br /> 7421 AA <br /> LEADED <br /> OAS X X <br /> UNL GAS }{ X X <br /> x <br /> DIESEL X X <br /> KE,ROSEN$ X X <br /> UNK FUEL x x x <br /> x x <br /> PROD. OIL x X <br /> CHLOR- <br /> SOLVENTS X X <br /> NON'CHL.OR <br /> SOLVENTS X X X A, <br /> WASTE% <br /> USED OIL X X x xAll ; <br /> X x <br /> in analyses aMethods are designated EPA methods described in EPA SW 846, Third Edition. Those methods not found <br /> detectiba limbs of Carp tee below. <br /> Refer to the SWRCB LUFT Feld Manual", Appendix A-20, Table 3.5 for <br /> Initial EvOluAtion and Investigation of(gasoline for the waste and motor oil de[ec-Regional Sand Staff Recommendations for <br /> Detactiop,Llmita U. <br /> that rein below the MCI. MX or Allowable Limit of the contaminant in question will be accepted, <br /> however labors" shall uWIU the moat conservative method <br /> LABORATORY ANALYSES TERMINOLOGY: <br /> TPH-G Total Petroleum Hy&ocarboa, Gaw ae, GC/FM (3030) 8015 mod or GAMS 8260 <br /> TPH-D Total Petroleum Hydrocarbon, Diesel, GGFID (3$50), 8015 mod or 0 . 8260 <br /> BTx & E Bemmne, Toluene, Xyleas & Ethyl Benzene, OGPID 8020 or GClM3 8260 <br /> CL HC C4[lorinated Hydrocarbon, OCIFI$>7 8010, GQMS 8240 <br /> TOTAL LEAD Total lead, AA 7420, AA 7421 Of ICP.AES 5010 <br /> EDB Ethylene dlbromido (DHS-AB 1803), GQMS 5240 (DHS-LLrn <br /> GC-1711) Ow Chromatography, Flamm Ionization Detection <br /> ICAP or AA Inducrfvely Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption <br /> PCH Spectrometry 7000. Metalst Cedmium, ChMthlum III and 'VI, Lead, Zinc and NIckel. <br /> Method 3050 Pplyehlorinated Biphenyls, GC/MS 82M or 8080 <br /> Acid digestion <br /> Method 3540 soahlet sample preparation <br /> Method 3550 sonication sample preparation, uuaotlon method <br /> Method SOW Purge ad trap sample preparation <br /> QA/QC Quality Assunnoe/Qu Ety Control <br /> Notes: To avoid false positive detection of benzene, bedzene•free solvents are to be used. Fused c ptlliry rpittmtts fro <br /> preferred to packed columns; a packed column may be used as a '6t'st cut*with "dirty" samples or once the hydrocarbons <br /> have been Character'sed and proper QA/AC is followed. <br /> For Drinking watertoctJo , <br /> series because the dotectioEPA recommends that the 500 series for volatile organics be used is preference to the b00 <br /> a limits are lower and the QA/QC is better. Samples exhibiting any level f heavy metal <br /> contamination may require further analysis. PHS-F,IM recommends holding these sampler until disposal is indicted <br /> EH 23 048 (Revised 7/10192) ?Age <br />