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MINIMUM VERIFICATION LABORATORY ANALYSIS <br /> TA1-IK TANK TPH-G TPH-D BTX & E CL HC ZO <br /> AL EDB METALS PCB <br /> # CONTENTS 8015 8015 8020 8010 D ICRP/ 8270 <br /> 8260 8260 8260 8240 8240 AES or 8080 <br /> 7421 AA <br /> LEADED <br /> GAS X X X X <br /> UNL GAS X X <br /> DIESEL X X <br /> KEROSENE X X <br /> UNK FUEL X X X X X <br /> PROD. OIL X X <br /> CHLOR. <br /> SOLVENTS X X <br /> NONCHLOR <br /> SOLVENTS X X X <br /> WASTE\ <br /> USED OIL X X X X X X <br /> All analyses methods are designated EPA methods described in EPA SW 846, Third Edition. Those methods not found in <br /> SW 846, are specifically noted below. Refer to the "SWRCB LUFT FieId Manual",Appendix A-20, Table 3-5 for detection <br /> Iimits of motor vehicle fuels (gasoline and diesel). Refer to 1-2-3 "Regional Board Staff Recommendations for Initis! <br /> Evaluation and Investigation of UST's" for the waste and motor oil detection Iimits. <br /> Detection. Limits that remain below the MCI:, STLC or Allowable Limit of the contaminant in question will be accepted, <br /> however laboratory shall utilize the most conservative method. <br /> LABORATORY ANALYSES TERMINOLOGY: <br /> TPH-G Total Petroleum Hydrocarbon, Gasoline, GC/FID (5030) 8015 mod or GC/MS 8260 <br /> TPH-D Total Petroleum Hydrocarbon, Diesel, GC/FID (3550), 8015 mod or GC/MS 8260 <br /> BTX & E Benzene, Toluene, Xylene & Ethyl Benzene, GC/PID 8020 or GC/MS 8260 <br /> CL HC Chlorinated Hydrocarbon, GC/HSD 8010, GC/MS 8240 <br /> TOTAL LEAD Total lead, AA 7420, AA 7421 or ICP-AES 6010 <br /> EDB Ethylene dibromide (DHS-AB 1803), GC/MS 8240 (DHS-Luh) <br /> GC-FID Lias Chromatography, Flame Ionization Detection <br /> ICRP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption <br /> Spectrometry 7000. Metals: Cadmium, Chromium III and VI, Lead, Zinc and Nickel. <br /> PCB Polychlorinated Biphenyls, GEMS 8270 or 8080 <br /> Method 3050 Acid digestion <br /> Method 3540 Soxhlet sample preparation <br /> Method 3550 Sonication sample preparation, extraction method <br /> Method 5030 Purge and trap sample preparation <br /> QA/QC Quality Assurance/Quality Control <br /> Notes_ To avoid false positive detection of benzene, benzene-free solvents are to be used. Fused capillary columns are <br /> preferred to packed columns; a packed column may be used as a "first cut" with "dirty" samples or once the hydrocarbons <br /> have been characterized and proper QA/AC is followed. <br /> For Drinking water sources, EPA recommends that the 500 series for volatile organics be used in preference to the 600 series <br /> because the detection limits are lower the QA/QC is better. <br /> EH 23 048 (Rev 4/8/91) Page 8 <br />