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Page 3 of 3 <br /> Spargero Analytical Laboratory Division <br /> Technology Mobile Laboratory Division <br /> Inc. Scientific Division <br /> With Automation in Mind <br /> EPA Method 625 <br /> GCMS Analysis Report <br /> Method Blank <br /> Attention: Mr. Jonathan Le Date Sampled: Jan 14, 1998 <br /> Precision Environet-Tech Date Received: Jan 15, 1998 <br /> 2040 E. Harding Way, Ste. B Date Analyzed: Jan 22, 1998 <br /> Stockton, CA 95205 Invoice#: 9003JAN98 <br /> Project#: Project Name: Neward Sierra Paper <br /> Client ID: Method Blank LAB ID: 9003-MB <br /> Matrix: Water Dilution: 1: 1 <br /> Name Amount Reporting Limit Units <br /> 55.) Hexachloroethane ND 10 ug/I <br /> 56.) Indeno(1,2,3-cd) Pyrene ND 10 ug/l <br /> 57.) Isophorone ND 10 ug/1 <br /> 58.) N -Nitroso-Di-Propylamine ND 10 ug/I <br /> 59.) N- Nitrosodiphenylamine ND 10 ug/I <br /> 60.) Naphthalene ND 10 ug/1 <br /> 61.) Nitrobenzene ND 10 ug/1 <br /> 62.) Pentachlorophenol ND 50 ug/I <br /> 63.) Phenanthrene ND 10 ug/1 <br /> 64.) Phenol ND 10 ug/I <br /> 65.) Pyrene ND 10 ugll <br /> Surrogate% Recovery 2 - Fluorophenol= 55% <br /> Surrogate% Recovery Phenol -d6= 71% <br /> Surrogate % Recovery Nitrobenzene-d5= 83% <br /> Surrogate% Recovery 2-Fluorobiphenyl = 84% <br /> Surrogate % Recovery 2,4,6-Tribromophenol = 82% <br /> Surrogate% Recovery Terphenyl -d14= 111% <br /> ppb=parts per billion=ugll=micrpgrems per Iger <br /> ppm=parts per million=ug/ml=mx;Wams per milliliter <br /> ND=Not DetWW Compo IM(s)may bo present at concentrations below the reporting limit. <br /> Jan 29, 1998 <br /> R.L.James,Principal Chemist Date Reported <br /> SPARGER TECHNOLOGY ANALYTICAL LABORATORY,INC.IS CERTIFIED BY THE STATE OF CALIFORNIA <br /> DEPARTMENT OF HEALTH SERVICES AS A HAZARDOUS WASTE TESTING LABORATORY <br /> (Certification No.1614) <br /> 625mbw <br /> 3050 Fite Circle, Suite 112 • Sacramento, California 95827 is (916) 362-8947 is FAX (916) 362-0947 <br />