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Spargero Analytical Laboratory Division <br /> Technology Mobile Laboratory Division <br /> Inc. Scientific Division <br /> ,vrth Automation in Mind <br /> EPA Method 625 GCMS Laboratory Control Spike (LCS) and <br /> Laboratory Control Spike Duplicate (LCSD) <br /> Attention: Mr. Jonathan Le Date Sampled: Jan 14, 1998 <br /> Precision Environet-Tech Date Received: Jan 15, 1998 <br /> 2040 E. Harding Way, Ste. B Date Analyzed: Jan 22, 1998 <br /> Stockton, CA 95205 Invoice#: 9003JAN98 <br /> Project#: Project Name: Neward Sierra Paper <br /> Client ID: LCS/LCSD LAB ID: 9003-LCS <br /> 9003-LCSD <br /> Matrix: Water Dilution: <br /> UNITS= ug/I <br /> Sample Spike(ppb) LCS LCSD QC Limits <br /> Compound Conc Added LCS LCSD % Rec % Rec RPD RPD % Rec <br /> Phenol ND 200 130 131 65% 66% 1% 42 12-89 <br /> 2-Chlorophenol ND 200 144 139 72% 70% 4% 40 27-123 <br /> 1, 4-Dichlorobenzene ND 100 71 67 71% 67% 6% 28 36-120 <br /> N-Nitroso-di-n-propylamine ND 100 92 89 92% 89% 3% 38 41-116 <br /> 1, 2, 4-Trichlorobenzene ND 100 64 66 64% 66% 3% 28 39-120 <br /> 4-Chloro-3-Methylphenol ND 200 171 176 86% 88% 3% 42 23-97 <br /> Acenaphthene ND 100 99 99 99% 99% 0% 31 46-118 <br /> 4-Nitrophenol ND 200 152 155 76% 78% 2% 50 10-120 <br /> 2, 4-Dinitrotoluene ND 100 94 92 94% 92% 2% 38 24-120 <br /> Pentachlorophenol ND 200 159 164 80% 82% 3% 50 9-150 <br /> Pyrene ND 100 116 113 116% 113% 3% 31 26-127 <br /> ppb=parts per billion=ugll=m"rams per liter <br /> ppm=parts per million=uglml=micrograms per milliliter <br /> NO=Not Detected. Compounds)may be present at concentrations below the detection limit. <br /> Jan 29, 1998 <br /> R.L. James, Principal Chemist Date Reported <br /> SPARGER TECHNOLOGY ANALYTICAL LABORATORY.INC.IS CERTIFIED BY THE STATE OF CALIFORNIA <br /> DEPARTMENT OF HEALTH SERVICES AS A HAZARDOUS WASTE TESTING LABORATORY <br /> comfl.d.No.1614) <br /> 6251csw <br /> 3050 Fite Circle, Suite 112 is Sacramento, California 95827 • (916) 362-8947 FAX (916) 362-0947 <br />