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Spargero Analytical Laboratory Division <br /> Mobile Laboratory Division <br /> Technology, Inc. Scientific Division <br /> h ur�n In Mina <br /> EPA Method 625 GCMS Analysis Report <br /> Matrix Spike (MS) and Matrix Spike Duplicate (MSD) <br /> Attention: Mr. Jonathan Le Date Sampled: Jan 14, 1998 <br /> Precision Environet-Tech Date Received: Jan 15, 1998 <br /> 2040 E. Harding Way, Ste. B Date Analyzed: Jan 22, 1998 <br /> Stockton, CA 95205 Invoice#: 9003JAN98 <br /> Project#: Project Name: Neward Sierra Paper <br /> Client ID: MS/MSD (Batch) LAB ID: 9002-012MS <br /> 9002-012MSD <br /> Matrix: Water Dilution: <br /> Units= uglml <br /> Sample Spike (ppm) MS % MSD % QC Limits <br /> Compound Conic Added MS MSD Rec Rec. RPb RPD % Rec <br /> Phenol ND 200 145 151 73% 76% 4% 35 26-90 <br /> 2-Chlorophenol ND 200 132 146 66% 73% 10% 50 25-102 <br /> 1, 4-Dichlorobenzene ND 100 63 70 63% 70% 11% 27 28-104 <br /> N-Nitroso-di-n-propylamine ND 100 92 101 92% 101% 9% 38 41-126 <br /> 1, 2, 4-Trichlorobenzene ND 100 63 70 63% 70% 11% 23 26-103 <br /> 4-Chloro-3-Methylphenol ND 200 180 186 90% 93% 3% 33 26-103 <br /> Acenaphthene ND 100 96 98 96% 98% 2% 19 31-137 <br /> 4-Nitrophenol ND 200 164 158 82% 79% 4% 50 11-114 <br /> 2, 4-Dinitrotoluene ND 100 84 88 84% 88% 5% 47 28-89 <br /> Pentachlorophenol ND 200 116 116 58% 58% 0% 47 17-109 <br /> Pyrene ND 100 89 87 89% 87% 2% 36 35-142 <br /> ppb=parts per billion=ugll=micrograms par liter <br /> ppm=parts per million=uglml=micrograms per milliliter <br /> NO=Not Detected Compountlls)may be present at concentrations below the detection limit. <br /> Jan 29, 1998 <br /> R. L.James, Principal Chemist Date Reported <br /> SPARGER TECHNOLOGY ANALYTICAL LABORATORY.INC.IS CERTIFIED BY THE STATE OF CALIFORNIA <br /> DEPARTMENT OF HEALTH SERVICES AS A HAZARDOUS WASTE TESTING LABORATORY <br /> (Candication No 1614) <br /> 625msw <br /> 3050 Fite Circle. Suite 112 • Sacrorn-=nto, California 95827 • (916) 362-8947 is FAX (916) 362-0947 <br />