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110 Second Avenue South,#D7,Pacheco,CA 94553 <br /> McCAWBEL •ANALYTICAL INC. Telephone:510-799-1620 Fax:510-798-1622 <br /> E-mail:main@mccampbell.com <br /> - <br /> Advanced GeoEnvironmeptal Client Project IDit Date Sampled: 07/14/97:Hickinbotha <br /> 1803 West March Lane,Ste A Brothers Date Received:07/11/97 <br /> Stockton,CA 95207 Client Contact:Bill Little Date Extracted:07/11/97 <br /> Client P.O: Date Analyzed:07/11/97 <br /> CAM/CCR 17 Metals* <br /> EPA methods 6010!200.7;747W7471/245.1/245.3 Hg);7060/206.2(As);77401270.2(Se);78411279.2(TI);239.2(Pb,water matrix) <br /> Lab ID 79492 <br /> Reporting Limit <br /> Client ID PB7-5' <br /> Matrix S S W STLC, <br /> Extracdoe TTLC TTLC TTLC TCLP <br /> Compound Concentration* mg/kg rrtglL mg/L <br /> Antimony(Sb) ND 2.5 0.05 0.05 <br /> Arsenic(As) 13 2.5 0.005 0.25 <br /> Barium(Ba) 160 1.0 0.05 0.05 <br /> Beryllium(Be) ND 0.5 0.004 0.01 <br /> Cadmium(Cd) ND 0.5 0.005 0.01 <br /> Chromium(Cr) 36 0.5 0.005 0.05 <br /> Cobalt(Co) 11 2.0 0.05 0.05 <br /> Copper(Cu) 25 2.0 0.05 0.05 <br /> Lead(Pb) 6.1 3.0 0.005 0.2 <br /> Mercury(Hg) ND 0.06 0.0008 0.0008 <br /> Molybdenum(Mo) ND 2.0 0.05 0.05 <br /> Nickel(Ni) 26 2.0 0.05 0.05 <br /> Selenium(Se) ND 2.5 0.005 0.25 <br /> Silver(Ag) ND 1.0 0.01 0.05 <br /> Thallium(TI) ND 0.5 0.001 0.5 <br /> Vanadium(V) 51 2.0 0.05 0.05 <br /> Zinc(Zn) 48 1.0 0.05 0.05 <br /> %Recovery Surrogate 103 <br /> Comments <br /> •water samples are reported in mgJL.,soil and sludge samples in mglkg,wipes in ug/wipe and all TCLP/STLC!SPLP extracts in mg/L <br /> ND means not detected above the reporting limit;N/A means surrogate not applicable to this analysis . <br /> °EPA extraction methods 131 l(TCLP),3010/3020(water,TTLC),3040(organic matriccs.TTLC),3050(solids,TTLC);STLC-CA Title 22 <br /> r surrogate diluted out of range <br /> `reporting limit raised due to matrix interference <br /> i) liquid sample that contains greater than -2 vol % sediment; this sediment is extracted with the liquid, in accordance with EPA <br /> medwelokiSies and can significantly effect reported metal concentrations. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />