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I 10 Second Avenue Soon(,ND7,Pacheco,CA 94553 <br /> McCAWBELL ANALYTICAL INC. Telephone:510-798-1620 Fax:510-798-1622 <br /> E-mail:maitt@mcewnpbell.com <br /> Date Sampled:07/10/97 <br /> Advanced GeoEavironmenttal Client Project ID:Hickinbothan <br /> 1803 West March Lane,Ste A Brothers Date Received:07/11/97 <br /> Stockton,CA 95207 Client Contact Bill Little Date Extracted:07/14-07/16197 <br /> Client P.O: Date Analyzed:07/16-07/17197 <br /> CAM I CCR 17 Metals* <br /> EPA methods 6010f200.7;7470f7471245.1245.5(11g);70601206.2(As):7740/270.2(Sch 7941/279.2(TI);239.2(Pb,water matrix) <br /> Lab ID 78492 <br /> Reporting Limit <br /> Client ID PB7-5' <br /> Matrix S S w <br /> STLC, <br /> Extraction° STLC TTLC TTLC TCLP <br /> Compound Concentration* mg/kg mg/L mg/L <br /> Antimony(Sb) ND 2.5 0.05 0.05 <br /> Arsenic(As). ND 2.5 0.005 0.25 <br /> Barium(Ba) 12 1.0 0.05 0.05 <br /> Beryllium(Be) ND 0.5 0.004 0.01 <br /> Cadmium(Cd) ND 0.5 0.005 0.01 <br /> Chromium(Cr) ND 0.5 0.005 0.05 <br /> Cobalt(Co) 0.60 2.0 0.05 0.05 <br /> Copper(Cu) 0.22 2.0 0.05 0.05 <br /> Lead(Pb) ND 3.0 0.005 0.2 <br /> Mercury(Hg) ND 0.06 0.0008 0.0008 <br /> Molybdenum(Mo) ND 2.0 0.05 0.05 <br /> Nickel(Ni) 0.60 2.0 0.05 0.05 <br /> Selenium(Se) ND 2.5 0.005 0.25 <br /> Silver(Ag) ND 1.0 0.01 0.05 <br /> Thallium(TI) ND 0.5 0.001 0.5 <br /> Vanadium(V) 0.72 2.0 0.05 0.05 <br /> Zinc(Zn) 0.054 1.0 0.05 0.05 <br /> %Recovery Surrogate NA <br /> Comments <br /> *water samples are reported in mg/L,soil and sludge samples in mgft.wipes in ug/wipe and all TCLP/STLC/SPLP extracts in mg/L <br /> ND means not detected above the reporting limit;NIA means surrogate not applicable to this analysis <br /> 'EPA extraction methods 131((TCLP),3010/3020(water,TTLC),3040(organic matrices.TTLC),3050(solids,TTLC);STLC-CA Title 22 <br /> 0 surrogate diluted out of range <br /> •reporting limit raised due to matrix interference <br /> i) liquid sample that contains greater than 2 vol. % sediment; this sediment is extracted with the liquid, in accordance with EPA <br /> Te 'es and can significantly effect reported metal concentrations. <br /> DHS Certification No. 1644 _Edward Hamilton,Lab Director <br />