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Blank Spike/Blank Spike Duplicate Summary Page 2 of 3 <br /> Job Number: C31148 <br /> Account: ENCOCALA Encon Solutions, Inc. <br /> Project: 1145 S. Aurora Street-Stockton, CA <br /> Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch <br /> VL919-BS L29097.1) 1 12/02/13 XB n/a n/a VL919 <br /> VL919-BSD 1-29098.13 1 12/02/13 XB n/a n/a VL919 <br /> iv <br /> The QC reported here applies to the following samples: Method: SW846 8260B <br /> C31148-2, C31148-4, C31148-6, C31148-8, C31148-10, C31148-12, C31148-14, C31148-16 <br /> Spike BSP BSP BSD BSD Limits <br /> CAS No. Compound ug/kg ug/kg % ug/kg % RPD Rec/RPD <br /> 591-78-6 2-Hexanone 160 134 84 121 76 10 68-139/24 <br /> 87-68-3 H exachlorobutadiene 40 39.8 100 36.7 92 8 81-126/32 <br /> 98-82-8 Isopropylbenzene 40 37.8 95 34.9 87 8 81-122/22 <br /> 99-87-6 p-Isopropyltoluene 40 35.7 89 32.8 82 8 81-121/23 <br /> 108-10-1 4-Methyl-2-pentanone 160 163 102 149 93 9 74-136/23 <br /> 74-83-9 Methyl bromide 40 41.2 103 39.0 98 5 82-124/20 <br /> 74-87-3 Methyl chloride 40 35.0 88 33.1 83 6 60-132/26 <br /> 74-95-3 Methylene bromide 40 40.7 102 38.9 97 5 82-120/20 <br /> 75-09-2 Methylene chloride 40 40.3 101 39.0 98 3 75-119/20 <br /> 78-93-3 Methyl ethyl ketone 160 150 94 142 89 5 71-130/22 <br /> 1634-04-4 Methyl Tert Butyl Ether 40 40.2 101 38.2 96 5 79-127/19 <br /> 91-20-3 Naphthalene 40 35.9 90 34.5 86 4 78-125/23 <br /> 103-65-1 n-Propylbenzene 40 33.5 84 31.0 78*a 8 79-124/22 <br /> 100-42-5 Styrene 40 39.1 98 37.3 93 5 83-122/21 <br /> 994-05-8 Tert-Amyl Methyl Ether 40 40.1 100 38.8 97 3 80-127/20 <br /> 75-65-0 Tert Butyl Alcohol 200 196 98 179 90 9 65-144/23 <br /> 630-20-6 1,1,1,2-Tetrachloroethane 40 38.8 97 36.7 92 6 82-123/21 <br /> 71-55-6 1,1,1-Trichloroethane 40 43.0 108 39.3 98 9 79-129/21 <br /> 79-34-5 1,1,2,2-Tetrachloroethane 40 34.0 85 31.7 79 7 77-126/20 <br /> 79-00-5 1,1,2-Trichloroethane 40 36.0 90 34.1 85 5 79-123/20 <br /> 87-61-6 1,2,3-Trichlorobenzene 40 37.2 93 35.8 90 4 81-122/26 <br /> 96-18-4 1,2,3-Trichloropropane 40 35.4 89 33.5 84 6 79-122/24 <br /> 120-82-1 1,2,4-Trichlorobenzene 40 36.8 92 35.2 88 4 81-121/26 <br /> 95-63-6 1,2,4-Trimethylbenzene 40 37.2 93 34.5 86 8 82-121/24 <br /> 108-67-8 1,3,5-Trimethylbenzene 40 38.3 96 35.5 89 8 81-123/23 <br /> 127-18-4 Tetrachloroethylene 40 41.2 103 38.1 95 8 80-125/25 <br /> 108-88-3 Toluene 40 38.8 97 36.3 91 7 80-117/21 <br /> 79-01-6 Trichloroethylene 40 43.3 108 39.7 99 9 81-122/20 <br /> 75-69-4 Trichlorofluoromethane 40 39.4 99 36.4 91 8 77-133/22 <br /> 75-01-4 Vinyl chloride 40 37.1 93 34.5 86 7 71-133/23 <br /> 1330-20-7 Xylene(total) 120 114 95 106 88 7 81-122/22 <br /> CAS No. Surrogate Recoveries BSP BSD Limits <br /> 1868-53-7 Dibromofluoromethane 88% 89% 70-130% <br /> * = Outside of Control Limits. <br /> No 54 of 80 <br /> 8.a.r-.C::tJTF=S;T <br /> C31148 `...--I- <br />