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Blank Spike/Blank Spike Duplicate Summary Page 1 of 3 <br /> Job Number: C31148 <br /> Account: ENCOCALA Encon Solutions, Inc. <br /> Project: 1145 S. Aurora Street-Stockton, CA <br /> Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch <br /> VL919-BS L29097.1) 1 12/02/13 XB n/a n/a VL919 <br /> VL919-BSD 1-29098.13 1 12/02/13 XB n/a n/a VL919 <br /> iv <br /> The QC reported here applies to the following samples: Method: SW846 8260B <br /> C31148-2, C31148-4, C31148-6, C31148-8, C31148-10, C31148-12, C31148-14, C31148-16 <br /> Spike BSP BSP BSD BSD Limits <br /> CAS No. Compound ug/kg ug/kg % ug/kg % RPD Rec/RPD <br /> 67-64-1 Acetone 160 144 90 133 83 8 62-130/24 <br /> 71-43-2 Benzene 40 42.4 106 39.9 100 6 81-119/20 <br /> 108-86-1 Bromobenzene 40 36.3 91 34.4 86 5 79-120/22 <br /> 74-97-5 Bromochloromethane 40 41.0 103 39.9 100 3 81-120/19 <br /> 75-27-4 Bromodichloromethane 40 38.8 97 37.1 93 4 79-124/20 <br /> 75-25-2 Bromoform 40 39.6 99 37.0 93 7 76-128/21 <br /> 104-51-8 n-Butylbenzene 40 36.5 91 33.5 84 9 79-123/26 <br /> 135-98-8 sec-Butylbenzene 40 35.6 89 32.5 81 9 77-122/24 <br /> 98-06-6 tert-Butylbenzene 40 35.5 89 33.1 83 7 77-121/23 <br /> 108-90-7 Chlorobenzene 40 36.2 91 34.1 85 6 82-121/20 <br /> 75-00-3 Chloroethane 40 35.8 90 33.2 83 8 80-126/21 <br /> 67-66-3 Chloroform 40 39.8 100 37.9 95 5 82-123/20 <br /> 95-49-8 o-Chlorotoluene 40 35.9 90 33.2 83 8 78-125/25 <br /> 106-43-4 p-Chlorotoluene 40 32.5 81 30.6 77 6 75-125/26 <br /> 56-23-5 Carbon tetrachloride 40 44.5 111 40.4 101 10 82-127/22 <br /> 75-34-3 1,1-Dichloroethane 40 38.6 97 36.4 91 6 80-123/20 <br /> 75-35-4 1,1-Dichloroethylene 40 42.2 106 39.1 98 8 76-123/19 <br /> 563-58-6 1,1-Dichloropropene 40 44.3 111 40.3 101 9 79-123/20 <br /> 96-12-8 1,2-Dibromo-3-chloropropane 40 31.4 79 29.7 74 6 64-133/23 <br /> 106-93-4 1,2-Dibromoethane 40 36.8 92 34.7 87 6 80-120/20 <br /> 107-06-2 1,2-Dichloroethane 40 38.6 97 36.8 92 5 76-132/21 <br /> 78-87-5 1,2-Dichloropropane 40 39.8 100 37.8 95 5 80-121/20 <br /> 142-28-9 1,3-Dichloropropane 40 35.2 88 33.4 84 5 78-120/20 <br /> 108-20-3 Di-Isopropyl ether 40 36.2 91 34.5 86 5 78-126/19 <br /> 594-20-7 2,2-Dichloropropane 40 41.8 105 38.3 96 9 77-132/22 <br /> 124-48-1 Dibromochloromethane 40 37.9 95 36.4 91 4 76-121/21 <br /> 75-71-8 Dichlorodifluoromethane 40 26.1 65 23.8 60 9 51-135/23 <br /> 156-59-2 cis-1,2-Dichloroethylene 40 42.6 107 40.2 101 6 79-123/20 <br /> 10061-01-5 cis-1,3-Dichloropropene 40 42.1 105 40.7 102 3 81-124/21 <br /> 541-73-1 m-Dichlorobenzene 40 34.6 87 32.4 81 7 79-123/23 <br /> 95-50-1 o-Dichlorobenzene 40 33.9 85 32.3 81 5 79-124/22 <br /> 106-46-7 p-Dichlorobenzene 40 37.2 93 35.2 88 6 79-123/22 <br /> 156-60-5 trans-l,2-Dichloroethylene 40 43.8 110 41.0 103 7 78-120/19 <br /> 10061-02-6 trans-l,3-Dichloropropene 40 35.2 88 33.8 85 4 81-123/22 <br /> 100-41-4 Ethylbenzene 40 39.0 98 36.2 91 7 80-119/21 <br /> 637-92-3 Ethyl tert-Butyl Ether 40 40.6 102 39.7 99 2 75-132/21 <br /> * = Outside of Control Limits. <br /> No 53 of 80 <br /> 8.a.r-.C::tJTF=S;T <br /> C31148 `...--I- <br />